Organic derivatives of alkylene dithiophosphates part III:: Synthesis and properties of 2-(p-nitrophenyl) and 2-(p-nitrobenzoyl) derivatives of alkylene dithiophosphates

被引：6
|
作者：
Sharma, CS [1 ]
Sharma, MK [1 ]
Nagar, PN [1 ]
机构：
[1] Univ Rajasthan, Dept Chem, Jaipur 302004, Rajasthan, India
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2002年 / 177卷 / 04期
关键词：
IR; NMR spectra; O; O '-alkylene dithiophosphates; p-bromonitrobenzene; p-O; O '-alkylene dithiophosphato-(S)-nitro-benzene; p-nitrobenzoyl chloride;
D O I：
10.1080/10426500210659
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Reactions of p-bromonitrobenzene and p-nitrobenzoyl chloride with ammonium salt of alkylene dithiophosphates ((OGOPS(2)NH(4): G = -CMe2CMe2-, -CH2CMe2CH2-, -CMe2CH2CHMe-, -CH2CH2 CHMe-) in 1:1 molar ratio in refluxing benzene solution yields: non-volatile yellow colored solids and red colored viscous liquids respectively of the type OGOP(S)SR (R = -C6H4NO2, (O)CC6H4NO2) which are monomeric in nature. The newly synthesized complexes have been characterized by physico-chemical and spectroscopic techniques (M.W, IR, NMR [H-1 and P-31]). On the basis of above studies, the formation of P-S-C and P-S-C(O) chemical bonds has been established.
引用
收藏
页码：981 / 987
页数：7
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