One step preparation and 1,3-dipolar cycloadditions of (S)-5-hydroxymethyl-1-pyrroline N-oxide

被引：30
|
作者：
Closa, M [1 ]
deMarch, P [1 ]
Figueredo, M [1 ]
Font, J [1 ]
机构：
[1] UNIV AUTONOMA BARCELONA,DEPT QUIM,BELLATERRA 08193,BARCELONA,SPAIN
来源：
TETRAHEDRON-ASYMMETRY | 1997年 / 8卷 / 07期
关键词：
D O I：
10.1016/S0957-4166(97)00042-6
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The cyclic nitrone Ib has been prepared in enantiomerically pure form by direct oxidation of L-(+)-prolinol with dimethyldioxirane. A complete diastereoface differentiation has been observed in the 1,3-dipolar cycloaddition reaction of this nitrone to several 1,2-disubstituted electron deficient olefins. (C) 1997 Elsevier Science Ltd.
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收藏
页码：1031 / 1037
页数：7
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