Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)

被引：0
|
作者：
Okio, Coco K. Y. A. [1 ]
Speziali, Nivaldo L. [2 ]
机构：
[1] Univ Nacl Colombia, Dept Quim, Bogota, Colombia
[2] Univ Fed Minas Gerais, Dept Fis, ICEx, Belo Horizonte, MG, Brazil
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词：
D O I：
10.1107/S1600536809018522
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The crystal structure of the title compound, [Sn(C(5)H(10)NS(2))(4)], was originally determined by Harreld & Schlemper [Acta Cryst. (1971), B27, 1964-1969] using intensity data estimated from Weissenberg films. In comparison with the previous refinement, the current redetermination reveals anisotropic displacement parameters for all non-H atoms, localization of the H atoms, and higher precision of lattice parameters and interatomic distances. The complex features a distorted S(6) octahedral coordination geometry for tin and a cis disposition of the monodentate dithiocarbamate ligands.
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收藏
页码：M675 / U736
页数：8
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