Sonochemical synthesis of carbon supported Sn nanoparticles and its electrochemical application

被引:4
|
作者
Anandan, Sambandam [1 ,2 ]
Wu, Jerry J. [2 ]
机构
[1] Natl Inst Technol, Dept Chem, Nanomat & Solar Energy Convers Lab, Tiruchirappalli 620015, India
[2] Feng Chia Univ, Dept Environm Engn & Sci, Taichung 40724, Taiwan
关键词
Sonochemical synthesis; Vulcan carbon; Tin nanoparticles; X-ray diffraction; Electrochemical properties; FUEL-CELL; ELECTROCATALYST; ULTRASOUND; REDUCTION; NANOTUBES; CATALYSTS;
D O I
10.1016/j.ultsonch.2014.02.018
中图分类号
O42 [声学];
学科分类号
070206 ; 082403 ;
摘要
A sonochemical approach was employed to prepare Vulcan carbon XC-72R supported by Sn nanoparticles at room temperature in the presence of ethylene glycol. The reduction of metallic Sn ion and ethylene glycol takes place and in turn the glycolate ion as formed acts as a stabilizing agent. Transmission electron microscope, X-ray diffraction, and X-ray photoelectron spectroscopy have illustrated that the metallic Sn nanoparticles are successfully embedded on the carbon. The significantly observed reduction over potential for oxygen reduction reaction displays a higher catalytic activity of carbon supported by Sn nanoparticles due to the large surface area of the modified electrode. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:1954 / 1957
页数:4
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