Solvent-free synthesis of chiral N,N′-disubstituted thioureas by 'just mixing' the reagents

被引：23
|
作者：
Vázquez, J
Bernès, S
Reyes, Y
Moya, M
Sharma, P
Alvarez, C
Gutiérrez, R
机构：
[1] Univ Autonoma Puebla, Fac Ciencias Quim, Lab Sintesis Complejos, Puebla 72001, Mexico
[2] Univ Autonoma Puebla, Inst Ciencias, Ctr Quim, Puebla 72000, Mexico
[3] Univ Nacl Autonoma Mexico, Inst Quim, Mexico City 04510, DF, Mexico
来源：
SYNTHESIS-STUTTGART | 2004年 / 12期
关键词：
chiral thioureas; green-chemistry; crystallographic analysis;
D O I：
10.1055/s-2004-829167
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The synthesis of new chiral thioureas 3a-f by using the ecofriendly solvent-free and microwave-assisted approaches is reported and. unexpectedly, in the former method by just mixing the starting materials the products are instantaneously obtained. The crystal structures for 3b. 3c and 3e are also reported.
引用
收藏
页码：1955 / 1958
页数：4
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