Effects of various polyoxyethylene sorbitan monooils (Tweens) and sodium dodecyl sulfate on reflux synthesis of copper nanoparticles

被引：39
|
作者：
Zhang, Xifeng
Yin, Hengbo [1 ]
Cheng, Xiaonong
Hu, Huifeng
Yu, Qi
Wang, Aili
机构：
[1] Jiangsu Univ, Sch Chem & Chem Engn, Zhenjiang 212013, Peoples R China
[2] Jiangsu Univ, Sch Mat Sci & Engn, Zhenjiang 212013, Peoples R China
来源：
MATERIALS RESEARCH BULLETIN | 2006年 / 41卷 / 11期
关键词：
metals; nanostructures; chemical synthesis; electron diffraction; x-ray diffraction;
D O I：
10.1016/j.materresbull.2006.04.008
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Size-controlled synthesis of phase pure Cu nanoparticles was carried out by using copper sulfate pentahydrate as a precursor, ascorbic acid as a reductant, Tweens and sodium dodecyl sulfate (SDS) as modifiers in an aqueous solution at 80 degrees C. The asprepared Cu nanoparticles were characterized by powder X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and Fourier transform infrared (FT-IR). The stabilizing effects of SIDS and Tweens on the Cu nanoparticles should be through the coordination between Cu nanoparticles and the respective sulfate group and oxygencontaining bond. The synergic effect of the composite SIDS and Tweens on Cu nanoparticles was different from those arising from the individuals. (c) 2006 Elsevier Ltd. All rights reserved.
引用
收藏
页码：2041 / 2048
页数：8
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