Synthesis of MCM-41 with High Manganese Content by Mechanochemical Pretreatment of the Starting Materials

被引：3

作者：

Iida, Takayuki ^{[1
]}

Sato, Mitsutaka ^{[2
]}

Liu, Zhendong ^{[1
]}

Numako, Chiya ^{[3
]}

Nakahira, Atsushi ^{[4
]}

Okubo, Tatsuya ^{[1
]}

Wakihara, Toru ^{[1
]}

机构：

[1] Univ Tokyo, Dept Chem Syst Engn, Bunkyo Ku, Tokyo 1138656, Japan

[2] Tohoku Univ, Inst Mat Res, Osaka Ctr, Naka Ku, Sakai, Osaka 5998531, Japan

[3] Chiba Univ, Grad Sch Sci, Inage Ku, Chiba 2638522, Japan

[4] Osaka Prefecture Univ, Grad Sch Engn, Dept Mat Sci, Naka Ku, Sakai, Osaka 5998531, Japan

来源：

CHEMISTRY LETTERS | 2014年 / 43卷 / 08期

关键词：

MESOPOROUS MOLECULAR-SIEVES; STRUCTURAL-PROPERTIES; CATALYTIC-ACTIVITY; OXIDATION; MN-MCM-41; SURFACE;

D O I：

10.1246/cl.140340

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Manganese-incorporated MCM-41 with high manganese content of Mn/(Mn + Si) = 9.2 mol % and BET specific surface area of 750 m(2) g(-1) was obtained by utilizing mechanochemical treatment. Clear differences in the state of manganese throughout the synthetic conditions were confirmed by various spectroscopic analyses.

引用

页码：1346 / 1348

页数：3

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