Synthesis, spectroscopic studies and crystal structure of (Et4N)(SnMe3)7(HASO4)4 • 2H2O

被引：17
|
作者：
Diassé-Sarr, A
Barry, AH
Jouini, T
Diop, L
Mahieu, B
Mahon, MF
Molloy, KC
机构：
[1] Univ Cheikh Anta Diop, Fac Sci & Tech, Dept Chim, Dakar, Senegal
[2] Fac Sci Tunis, Tunis 1060, Tunisia
[3] CPMC, Dept Chim, B-1348 Louvain, Belgium
[4] Univ Bath, Dept Chem, Bath BA2 7AY, Avon, England
来源：
JOURNAL OF ORGANOMETALLIC CHEMISTRY | 2004年 / 689卷 / 12期
关键词：
trimethvitin(IV); monohydrogen arsenate; spectroscopy; supramolecuar structure;
D O I：
10.1016/j.jorganchem.2004.03.033
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
On allowing tetraethylammonium dihydrogen arsenate dihydrate to react with trimethyltin chloride, the title compound has been obtained and characterized by infrared, Mossbauer and NMR techniques. Its crystal structure has been determined and consists of layers containing both corner sharing AsO4H tetrahedra and trans-O2SnC3 entities. It contains large cavities in which tetraethylamonium cations are located. (C) 2004 Elsevier B.V. All rights reserved.
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收藏
页码：2087 / 2091
页数：5
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