Study of free-radical copolymerization of acrylamide with 2-acrylamido-2-methyl-1-propane sulphonic acid

被引：1

作者：

Travas-Sejdic, J ^{[1
]}

Easteal, A ^{[1
]}

机构：

[1] Univ Auckland, Dept Chem, Auckland, New Zealand

来源：

JOURNAL OF APPLIED POLYMER SCIENCE | 2000年 / 75卷 / 05期

关键词：

free-radical copolymerization; monomer reactivity ratio; copolymer microstructure;

D O I：

10.1002/(SICI)1097-4628(20000131)75:5<619::AID-APP4>3.0.CO;2-E

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

The free-radical initiated synthesis of acrylamide-co-2-acrylamido-2-methyl-1-propane sulphonic acid (AAm-co-AMPS) was studied at 60 and 25 degrees C. The monomer reactivity ratios were evaluated using Fineman-Ross and Kelen-Tudos methods, based on elemental analysis of the copolymers and C-13-NMR experimental data. The detailed copolymer microstructure was derived from reactivity ratios using the conditional probability based on the terminal kinetic model for free-radical polymerization. The homopolymers and copolymers were characterized using H-1- and C-13-NMR, and Fourier transform infrared (FTIR) spectroscopic methods, and differential scanning calorimetry. (C) 2000 John Wiley & Sons, Inc.

引用

页码：619 / 628

页数：10

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