New method for benzo[a] pyrene analysis in plant material using subcritical water extraction

被引：23

作者：

Sushkova, Svetlana N. ^{[1
]}

Vasilyeva, Galina K. ^{[2
]}

Minkina, Tatjana M. ^{[1
]}

Mandzhieva, Saglara S. ^{[1
]}

Tjurina, Irina G. ^{[1
]}

Kolesnikov, Sergei I. ^{[1
]}

Kizilkaya, Ridvan ^{[3
]}

Askin, Tayfun ^{[4
]}

机构：

[1] Southern Fed Univ, Rostov Na Donu, Russia

[2] Russian Acad Sci, Inst Physicochem & Biol Problems Soil Sci, Pushchino 142292, Moscow Region, Russia

[3] Ondokuz Mayis Univ, Samsun, Turkey

[4] Ordu Univ, Ordu, Turkey

来源：

JOURNAL OF GEOCHEMICAL EXPLORATION | 2014年 / 144卷

基金：

俄罗斯基础研究基金会;

关键词：

Benzo[a]pyrene; Plants; Subcritical water extraction; Hexane extraction; POLYCYCLIC AROMATIC-HYDROCARBONS; PRESSURIZED LIQUID EXTRACTION; SUPERCRITICAL-FLUID EXTRACTION; HOT-WATER; ENVIRONMENTAL SOLIDS; PAHS; CHROMATOGRAPHY; MATRICES; SOILS;

D O I：

10.1016/j.gexplo.2014.02.018

中图分类号：

P3 [地球物理学]; P59 [地球化学];

学科分类号：

0708 ; 070902 ;

摘要：

A new method for benzo[a] pyrene (BaP) analyses in plant material was developed using subcritical water extraction followed by HPLC analyses of the extracts. BaP extraction efficiency was determined by spiking grass vegetation collected from a preserve in Rostov Oblast (Russia). BaP recoverywas optimal with a 30-min extraction by water in a special steel cartridge at 250 degrees C and 100 atm. More than 98% of the BaP was recovered from the plant material using subcritical water extraction, compared to 72% recovery by saponification of the sample with conventional hexane extraction. Other advantages of subcritical water extraction are the use of water as an environmentally friendly solvent instead of large volumes of organic solvents as well as a shorter analysis time. (C) 2014 Elsevier B. V. All rights reserved.

引用

页码：267 / 272

页数：6

共 50 条

[21] Extraction of antioxidants from winery wastes using subcritical water
Aliakbarian, Bahar
Fathi, Ali
Perego, Patrizia
Dehghani, Fariba
JOURNAL OF SUPERCRITICAL FLUIDS, 2012, 65 : 18 - 24
[22] Remediation of PAHs contaminated soil by extraction using subcritical water
Islam, Mohammad Nazrul
Jo, Young-Tae
Park, Jeong-Hun
JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2012, 18 (05) : 1689 - 1693
[23] Extraction of isoflavones from Puerariae lobata using subcritical water
Zhang, Hongguang
Liu, Shuhua
Li, Huaizhi
Xue, Fumin
Han, Shuxin
Wang, Liang
Cheng, Yan
Wang, Xiao
RSC ADVANCES, 2018, 8 (40): : 22652 - 22658
[24] Extraction of diesel from contaminated soil using subcritical water
Islam, Mohammad Nazrul
Park, Ha-Seung
Park, Jeong-Hun
ENVIRONMENTAL EARTH SCIENCES, 2015, 74 (04) : 3059 - 3066
[25] Extraction of diesel from contaminated soil using subcritical water
Mohammad Nazrul Islam
Ha-Seung Park
Jeong-Hun Park
Environmental Earth Sciences, 2015, 74 : 3059 - 3066
[26] Subcritical water extraction method for extracting formaldehyde in dried beancurd sticks
Yang Hai
Zhang Chun-Wei
Mo Yu-Lin
Liang Xiang-Hui
Lu Xiao-Hua
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2007, 35 (06) : 929 - 929
[27] SUBCRITICAL EXTRACTION AS SAMPLE TREATMENT METHOD FOR ANTIOXIDANT SCREENING OF VARIOUS PLANT EXTRACTS
Hohnova, Barbora
St'avikova, Lenka
Karasek, Pavel
Roth, Michal
CECE 2014: 11TH INTERNATIONAL INTERDISCIPLINARY MEETING ON BIOANALYSIS, 2014, : 236 - 239
[28] SOME NEW DATA ON THE DISTRIBUTION OF BENZO (A) PYRENE IN FRESH-WATER AND SEA-WATER
VELDRE, IA
ITRA, AR
PAALME, LP
BOGOVSKI, PA
CANCER DETECTION AND PREVENTION, 1982, 5 (02): : 161 - 174
[29] Phthalic acid and benzo[a]pyrene in soil–plant–water systems amended with contaminated sewage sludge
Christian Mougin
Frederic Dappozze
Agathe Brault
Christian Malosse
Jens Ejbye Schmidt
Najat Amellal-Nassr
Dominique Patureau
Environmental Chemistry Letters, 2006, 4 : 201 - 206
[30] A novel method for food particle production using subcritical water extraction: Ganoderma mushroom as a case example
Uzel, Ruhan Askin
Yaman, Unal Riza
JOURNAL OF SUPERCRITICAL FLUIDS, 2016, 111 : 74 - 82

← 1 2 3 4 5 →