An Efficient One-Pot Synthesis of 1,4-Oxathiane and 1,4-Thiomorpholine Derivatives

被引：16
|
作者：
Samzadeh-Kermani, Alireza [1 ]
机构：
[1] Univ Zabol, Dept Chem, Fac Sci, Zabol, Iran
来源：
SYNLETT | 2014年 / 25卷 / 13期
关键词：
cyclization; epoxides; heterocycles; multicomponent reaction; ring opening; OXIDE; ALKENES;
D O I：
10.1055/s-0034-1378277
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An efficient one-pot reaction of nitromethane, isothiocyanates, and three-membered heterocyclic rings (oxiranes and aziridines) for the synthesis of 1,4-oxathiane and 1,4-thiomorpholine derivatives is reported. This procedure is carried out in the presence of K2CO3 in DMF at 60 degrees C.
引用
收藏
页码：1839 / 1842
页数：4
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