Effect of mechanical grinding in argon and hydrogen atmosphere on microstructure of graphite

被引：12
|
作者：
Touzik, A.
Hentsche, M.
Wenzel, R.
Hermann, H.
机构：
[1] Leibniz Inst Solid State & Mat Res Dresden, D-01171 Dresden, Germany
[2] Tech Univ Dresden, Inst Phys Chem & Electrochem, D-01062 Dresden, Germany
来源：
JOURNAL OF ALLOYS AND COMPOUNDS | 2006年 / 421卷 / 1-2期
关键词：
nanostructures; high-energy ball milling; graphite; pore size distribution; hydrogen atmosphere;
D O I：
10.1016/j.jallcom.2005.08.090
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Structural transformations and amorphization of graphite upon high-energy ball-milling under argon and hydrogen atmosphere are studied. Nano-scale carbon particles were characterized by nitrogen adsorption measurements (BET surface area) and high-resolution transmission electron microscopy (HRTEM). The pore size distribution (PSD) was determined by the Dollimore-Heal analysis. Maxima on PSD curves can be attributed to nanoscale structures formed by exfoliated graphite sheets or stacks of graphite sheets. The pore volume for each kind of pores strongly depends on the milling atmosphere. In contrast to that the maximal contribution of ultra micropores to the total porosity reaches about 40 vol.% independently of the milling atmosphere. (c) 2005 Elsevier B.V All rights reserved.
引用
下载
收藏
页码：141 / 145
页数：5
相关论文
共 50 条
  • [21] Thermodynamic Simulation of Heating of Radioactive Graphite in Argon Atmosphere
    N. M. Barbin
    T. S. Kolbin
    D. I. Terent’ev
    S. G. Alekseev
    M. A. Spiridonov
    High Temperature, 2018, 56 : 694 - 701
  • [22] PREPARATION OF NANOCRYSTALLINE TIAL POWDER BY THE HDDR PROCESS USING MECHANICAL GRINDING IN A HYDROGEN ATMOSPHERE
    AOKI, K
    ITOH, Y
    MASUMOTO, T
    SCRIPTA METALLURGICA ET MATERIALIA, 1994, 31 (09): : 1271 - 1275
  • [23] Effect of stress graphitization on the microstructure and mechanical properties of graphite fibers
    Xue Lin-bing
    Wang Hao-jing
    Li Dong-feng
    NEW CARBON MATERIALS, 2006, 21 (03) : 243 - 247
  • [24] Effect of stress graphitization on the microstructure and mechanical properties of graphite fibers
    Key Laboratory of Carbon Materials, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001, China
    不详
    Xinxing Tan Cailiao, 2006, 3 (243-247):
  • [25] Effect of tin on microstructure and mechanical properties of compacted graphite iron
    Lyu, Y.
    Sun, Y.
    Liu, S.
    Zhao, J.
    INTERNATIONAL JOURNAL OF CAST METALS RESEARCH, 2015, 28 (05) : 263 - 268
  • [26] Transformation of graphite structure under mechanical grinding
    Belenkov E.A.
    Opalev S.V.
    Russian Physics Journal, 2006, 49 (8) : 822 - 827
  • [27] The influence of grinding atmosphere on nanocrystalline iron microstructure formation
    Novakova, A.A.
    Gvozdover, R.S.
    Kiseleva, T.Yu.
    Tarasov, B.P.
    Katsnelson, A.A.
    Poverkhnost Rentgenovskie Sinkhronnye i Nejtronnye Issledovaniya, 2002, (10): : 43 - 48
  • [28] The magnetic properties of Nd-Fe-B powders produced by mechanical grinding in hydrogen atmosphere
    Saito, T
    JOURNAL OF APPLIED PHYSICS, 1999, 85 (08) : 5687 - 5689
  • [29] EFFECT ON DISCHARGE OF THE HEAT-TREATMENT OF GRAPHITE FLUORIDE UNDER A HYDROGEN ATMOSPHERE
    KUMAGAI, N
    KAWAMURA, M
    HIROHATA, H
    TANNO, K
    CHONG, Y
    WATANABE, N
    JOURNAL OF APPLIED ELECTROCHEMISTRY, 1995, 25 (09) : 869 - 873
  • [30] The effect of deposition temperature on microstructure and mechanical properties of SiC coatings on graphite
    Jiabao Liu
    Zhaofeng Chen
    Pan Chai
    Qiang Wan
    Asim Shahzad
    Journal of the Australian Ceramic Society, 2022, 58 : 557 - 562
12345