Flow extraction spectrophotometric method for the determination of diclofenac sodium in pharmaceutical preparations

被引:35
|
作者
PerezRuiz, T
MartinezLozano, C
Sanz, A
SanMiguel, MT
机构
[1] Department of Analytical Chemistry, Fac. of Chem., University of Murcia, 30071, Murcia
关键词
diclofenac; flow-injection method; ion-pair extraction; Acridine Yellow; spectrophotometry;
D O I
10.1016/S0731-7085(97)00028-9
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The spectrophotometric determination of trace amounts of diclofenac was carried out by liquid-liquid extraction using acridine yellow with a flow system. The determination of diclofenac sodium in the range of 3-80 mu g ml(-1) was possible with a sampling frequency of 40 samples h(-1). The method was satisfactorily applied to the determination of diclofenac in pharmaceutical preparations. (C) 1997 Elsevier Science B.V.
引用
收藏
页码:249 / 254
页数:6
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