Since nuclear magnetic resonance (NMR) spectroscopy obtains a quantitative value on the basis of a nucleus, the quantitative NMR technique does not require an identical standard. For this reason, it is expected to be a universal quantitative method. Recently, the quantitative NMR method was adopted also as a regulating method. However, the quantification using an NMR requires a high-resolution balance in the sample preparation for accurate weighing of the mass of samples. This is the biggest problems to disseminate a quantitative NMR as a generally used method. In this paper, we discuss the quantitative NMR method using the internal standard solution in order to resolve the problem. We examined two methods of sample preparation: the gravimetric method and the volumetric method. The influence of the preparation method and condition was evaluated using a standard solution. Additionally, some organizations have used this method to measure the purity of a high-purity reference material for the validation of this standard solution method. The accuracy of the results was evaluated using an internal standard solution by the volumetric method, and measured at 1 % or less.
机构:
Purdue Univ, Dept Chem, W Lafayette, IN 47907 USAPurdue Univ, Dept Chem, W Lafayette, IN 47907 USA
Fedick, Patrick W.
Bain, Ryan M.
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Purdue Univ, Dept Chem, W Lafayette, IN 47907 USAPurdue Univ, Dept Chem, W Lafayette, IN 47907 USA
Bain, Ryan M.
Bain, Kinsey
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Purdue Univ, Dept Chem, W Lafayette, IN 47907 USAPurdue Univ, Dept Chem, W Lafayette, IN 47907 USA
Bain, Kinsey
Cooks, R. Graham
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Purdue Univ, Dept Chem, W Lafayette, IN 47907 USA
Purdue Univ, Ctr Analyt Instrumentat Dev, W Lafayette, IN 47907 USAPurdue Univ, Dept Chem, W Lafayette, IN 47907 USA
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Hop Calmette, Lab Toxicol & Genopathies, F-59045 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
Cartigny, Bernard
Azaroual, Nathalie
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Univ Lille 2, CNRS, UMR 8009, Lab Phys,Applicat RMN, F-59800 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
Azaroual, Nathalie
Imbenotte, Michel
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Univ Lille 2, Toxicol Lab, F-59800 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
Imbenotte, Michel
Mathieu, Daniel
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Urgences Resp & Reanimat Med, F-59 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
Mathieu, Daniel
Parmentier, Erika
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Urgences Resp & Reanimat Med, F-59 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
Parmentier, Erika
Vermeersch, Gaston
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Univ Lille 2, CNRS, UMR 8009, Lab Phys,Applicat RMN, F-59800 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
Vermeersch, Gaston
Lhermitte, Michel
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Univ Lille 2, Toxicol Lab, F-59800 Lille, France
Hop Calmette, Lab Toxicol & Genopathies, F-59045 Lille, FranceUniv Lille 2, Toxicol Lab, F-59800 Lille, France
机构:
Russian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
St Petersburg State Univ, Dept Nucl Phys Res Methods, St Petersburg 199034, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Nerinovski, Kirill
Yakimov, Alexander
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NRC Kurchatov Inst, Petersburg Nucl Phys Inst, Gatchina 188300, Russia
Peter Great St Petersburg Polytech Univ, St Petersburg 195251, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Yakimov, Alexander
Kulikova, Veronika
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Russian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Peter Great St Petersburg Polytech Univ, St Petersburg 195251, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Kulikova, Veronika
Svetlova, Maria
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Russian Acad Sci, Inst Cytol, St Petersburg 194064, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Svetlova, Maria
Solovjeva, Ljudmila
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Russian Acad Sci, Inst Cytol, St Petersburg 194064, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Solovjeva, Ljudmila
Khodorkovskiy, Mikhail
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Peter Great St Petersburg Polytech Univ, St Petersburg 195251, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Khodorkovskiy, Mikhail
Gambaryan, Stepan
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Russian Acad Sci, Sechenov Inst Evolutionary Physiol & Biochem, St Petersburg 194223, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Gambaryan, Stepan
Cunningham, Richard
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Univ S Alabama, Mitchell Canc Inst, Mobile, AL 36604 USARussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Cunningham, Richard
Migaud, Marie E.
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Univ S Alabama, Mitchell Canc Inst, Mobile, AL 36604 USARussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Migaud, Marie E.
Ziegler, Mathias
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机构:
Univ Bergen, Dept Biomed, N-5020 Bergen, NorwayRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Ziegler, Mathias
Nikiforov, Andrey
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机构:
Russian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
Peter Great St Petersburg Polytech Univ, St Petersburg 195251, RussiaRussian Acad Sci, Inst Cytol, St Petersburg 194064, Russia
机构:
Flinders Univ S Australia, Sch Chem & Phys Sci, Adelaide, SA 5042, AustraliaFlinders Univ S Australia, Sch Chem & Phys Sci, Adelaide, SA 5042, Australia
Johnston, Martin R.
Cooper, Peter D.
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机构:
Australian Natl Univ, Canberra Hosp, ANU Med Sch, Canc Res Lab, Canberra, ACT 2605, Australia
Vaxine Pty Ltd, Flinders Med Ctr, Adelaide, SA 5042, AustraliaFlinders Univ S Australia, Sch Chem & Phys Sci, Adelaide, SA 5042, Australia
Cooper, Peter D.
Petrovsky, Nikolai
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Vaxine Pty Ltd, Flinders Med Ctr, Adelaide, SA 5042, Australia
Flinders Med Ctr, Dept Endocrinol, Adelaide, SA 5042, AustraliaFlinders Univ S Australia, Sch Chem & Phys Sci, Adelaide, SA 5042, Australia