Temperature, heat and heat flow rate calibration of differential scanning calorimeters

被引:56
|
作者
Gmelin, E
Sarge, SM
机构
[1] Max Planck Inst Festkorperforsch, D-70569 Stuttgart, Germany
[2] Phys Tech Bundesanstalt, D-38116 Braunschweig, Germany
关键词
differential scanning calorimeters; calibration of DSC; calibration of temperature; heat calibration; heat flow rate calibration;
D O I
10.1016/S0040-6031(99)00424-4
中图分类号
O414.1 [热力学];
学科分类号
摘要
This contribution discusses basic problems and fundamental requirements for a universally applicable, unified and metrologically correct calibration of differential scanning calorimeters (DSC). The essential features of previously published recommendations of the German Society for Thermal Analysis (GEFTA) [see Hohne et al., Thermochim. Acta 160 (1990) 112; Cammenga et al., Thermochim. Acta 219 (1993) 333-343; Sarge et al., Thermochim. Acta 247 (1994) 129-168; J. Thermal Anal. 49 (1997) 1125-1134] developed for a correct and instrument-independent calibration of temperature, heat and heat flow rate of DSC, are outlined. (C) 2000 Elsevier Science B.V. All rights reserved.
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页码:9 / 13
页数:5
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