First synthesis and structure of sulfur-containing heterocycles fused to ferrocene

被引：12

作者：

Nagahora, N

Ogawa, S ^{[1
]}

Kawai, Y

Sato, R

机构：

[1] Iwate Univ, Fac Engn, Dept Chem Engn, Morioka, Iwate 0208551, Japan

[2] Kyoto Univ, Inst Chem Res, Kyoto 6110011, Japan

来源：

TETRAHEDRON LETTERS | 2002年 / 43卷 / 33期

关键词：

sulfur heterocycles; ferrocenes; X-ray crystal structures; electrochemistry;

D O I：

10.1016/S0040-4039(02)01172-3

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Synthesis of a stable pentathiepin fused to a single cyclopentadienyl ring of ferrocene was performed by treatment of the corresponding dithiastannole as a synthetic equivalent of unstable ferrocene 1,2-dithiol with a sulfur source. On the other hand, deprotection of the dithinstannole gave a novel tetrathiocin comprised of two ferrocene units. The single-crystal X-ray diffraction Studies revealed the unprecedented sulfur-containing heterocycles bound to ferrocene units. (C) 2002 Elsevier Science Ltd. All rights reserved.

引用

页码：5825 / 5828

页数：4

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