In Situ Synthesis of Nanostructured WC-Co Within Silica Gel Matrix

被引:3
|
作者
Thakur, Arpita Dalapati [1 ]
Chaudhuri, Mahua Ghosh [1 ]
Das, Gopes C. [1 ]
Dey, Rajib [2 ]
Mitra, Manoj K. [2 ]
Mukherjee, Siddhartha [2 ]
机构
[1] Jadavpur Univ, Sch Mat Sci & Nanotechnol, Kolkata 700032, India
[2] Jadavpur Univ, Met & Mat Engn Dept, Kolkata 700032, India
关键词
TUNGSTEN CARBIDE; FTIR; NANOCOMPOSITE; POWDERS; ROUTE;
D O I
10.1111/ijac.12048
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In situ reduction of tungstic acid and cobalt chloride by dextrose in silica gel resulted in co-deposition of tungsten carbide-cobalt (WC-Co) nanoparticles with different proportions of cobalt (5-15 wt % of WC). X-ray powder diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), scanning electron microscopy (SEM) and Fourier-transform infrared (FT-IR) spectroscopy have been used for characterizing these nanoparticles. WC-Co aggregates of 25-30nm size have been achieved, successfully.
引用
收藏
页码:582 / 589
页数:8
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