Polymorphs of 1,1-bis(4-hydroxyphenyl) cyclohexane and multiple Z′ crystal structures by melt and sublimation crystallization

被引：68

作者：

Sarma, Bipul ^{[1
]}

Roy, Saikat ^{[1
]}

Nangia, Ashwini ^{[1
]}

机构：

[1] Univ Hyderabad, Sch Chem, Hyderabad 500046, Andhra Pradesh, India

来源：

CHEMICAL COMMUNICATIONS | 2006年 / 47期

关键词：

D O I：

10.1039/b610323e

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Close packing conflict in a metastable polymorph of the pure title host (Z' = 2, melt crystal 1m) is resolved in the stable form (Z' = 1, sublimed crystal 1s) as O-H center dot center dot center dot O hydrogen bond changes to O-H center dot center dot center dot pi interaction. Melt crystallization and sublimation show a greater percentage of high Z' structures in CSD statistics.

引用

页码：4918 / 4920

页数：3

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