Synthesis of Tricyclic Diesters

被引：0
|
作者：
Makhmudova, E. K. [1 ]
Rasulova, R. A. [1 ]
Kadyrly, V. S. [1 ]
Ibragimova, M. J. [1 ]
机构：
[1] Natl Acad Sci Azerbaijan, Mammadaliyev Inst Petrochem Proc, Baku 1025, Azerbaijan
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2020年 / 56卷 / 10期
关键词：
saturated carboxylic acids; tricyclic ester; 8-propanoyloxytricyclodec-3-ene; catalyst; boron trifluoride– diethyl ether complex; tricyclic diesters;
D O I：
10.1134/S1070428020100292
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The addition of saturated monobasic C-3-C-5 carboxylic acids to unsaturated tricyclic ester, tricyclo[5.2.1.0(2,6)]dec-3-en-8-yl propanoate, in the presence of boron trifluoride-diethyl ether complex gave the corresponding tricyclic diesters in 76.8-88.5 wt % yield. The product structure was confirmed by IR and H-1 and C-13 NMR spectra. The synthesized diesters possess a pleasant odor and can be recommended for use as synthetic fragrance substances in perfumery.
引用
收藏
页码：1847 / 1849
页数：3
相关论文
共 50 条
  • [41] BIOMIMETIC SYNTHESIS OF TRICYCLIC DITERPENES
    BRYSON, TA
    MCELLIGOTT, LT
    SYNTHETIC COMMUNICATIONS, 1982, 12 (04) : 307 - 312
  • [42] Synthesis of a library of tricyclic azepinoisoindolinones
    Miller, Bettina
    Mao, Shuli
    Rosenker, Kara M. George
    Pierce, Joshua G.
    Wipf, Peter
    BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, 2012, 8 : 1091 - 1097
  • [43] Synthesis of the tricyclic core of halichlorine
    Hayakawa, I
    Arimoto, H
    Uemura, D
    CHEMICAL COMMUNICATIONS, 2004, (10) : 1222 - 1223
  • [44] Synthesis of Tricyclic Precursors of Cyclitols
    Aucktor, Johannes
    Anselmi, Chiara
    Brueckner, Reinhard
    Keller, Manfred
    SYNLETT, 2014, 25 (09) : 1312 - 1318
  • [45] Straightforward Synthesis of 1,2-Amino Phosphate Diesters and Application to the Synthesis of Novel 1,2-Amino Ether Diesters
    Elemine, Brahim Ould
    Besbes, Rafaa
    Ennigrou, Mohamed Rached
    SYNTHETIC COMMUNICATIONS, 2010, 40 (01) : 64 - 73
  • [46] STUDIES IN MASS SPECTROMETRY .13. STEREOSPECIFIC ELECTRON IMPACT INDUCED FRAGMENTATION PROCESSES IN SOME TRICYCLIC DIESTERS
    DEUTSCH, J
    MANDELBA.A
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1970, 92 (14) : 4288 - &
  • [47] One-pot synthesis of phosphonic acid diesters
    Munoz, A
    Hubert, C
    Luche, JL
    JOURNAL OF ORGANIC CHEMISTRY, 1996, 61 (17): : 6015 - 6017
  • [48] PYRROLIZIDINE ALKALOID ANALOGS - SYNTHESIS OF MACROCYCLIC DIESTERS OF (-)-PLATYNECINE
    RODGERS, M
    ROBINS, DJ
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1989, (12): : 2437 - 2439
  • [49] Ruthenium-catalyzed regioselective synthesis of dienol diesters
    Kabouche, A
    Kabouche, Z
    Bruneau, C
    Dixneuf, PH
    JOURNAL OF CHEMICAL RESEARCH-S, 1999, (04): : 249 - +
  • [50] SYNTHESIS OF POLYAMIDES ON THE BASIS OF ACTIVATED DIESTERS OF PYRIDINECARBOXYLIC ACIDS
    ZHUBANOV, BA
    LYUBCHENKO, NP
    VYSOKOMOLEKULYARNYE SOEDINENIYA SERIYA A, 1982, 24 (07): : 1474 - 1479
12345