Synthetic pathways to new hydrated sodium and lithium vanadium bronzes

被引：6

作者：

Sabbar, EM ^{[1
]}

de Roy, ME ^{[1
]}

Besse, JP ^{[1
]}

机构：

[1] Univ Blaise Pascal, LMI, ESA CNRS 6002, F-63177 Clermont Ferrand, France

来源：

JOURNAL OF SOLID STATE CHEMISTRY | 2000年 / 149卷 / 02期

关键词：

D O I：

10.1006/jssc.1999.8578

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Synthesis of new hydrated sodium vanadium and lithium vanadium bronzes has been investigated by reaction of VOSO4. 5H(2)O, VO(C5H7O2)(2), or V2O3 with compounds containing C-O bonds (such as acetates) and NaOH or LiOH solutions under refluxing conditions in aqueous media. These layered compounds are characterized by X-ray powder diffraction, IR, and TGA, Thermal treatment for temperatures higher than 310 and 450 degrees C for sodium vanadium bronzes and lithium vanadium bronzes, respectively, leads to well-known anhydrous bronzes Na0.33V2O5 and Li0.22V2O5. (C) 2000 Academic Press.

引用

页码：443 / 448

页数：6

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