Synthesis, characterization and complexation behavior investigations of novel bis- and tris-crown ethers

被引：0

作者：

Huang, Zhi Bin

Kim, Sung Hong

Chang, Seung Hyun ^{[1
]}

机构：

[1] Daegu Univ, Dept Chem, Kyongbuk 712714, South Korea

[2] Suzhou Univ, Coll Chem & Chem Engn, Suzhou 215006, Peoples R China

[3] Korea Basic Sci Inst, Daegu Ctr, Anal Res Div, Taegu 702701, South Korea

来源：

BULLETIN OF THE KOREAN CHEMICAL SOCIETY | 2006年 / 27卷 / 06期

关键词：

2-acryloyloxymethyl crown ether; aza-crown ether; bis-crown ether; tris-crown ether;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Novel bis- and tris-crown ethers were synthesized from 1-aza and diaza-crown ethers with 2-acryloyloxymethyl crown ethers through Michael addition. The synthesized bis- and tris-crown ethers were characterized by their elemental analyses, H-1-NMR, C-13-NMR, mass spectra, IR spectra, respectively. The complexation behavior of the bis- and tris-crown ethers with Li+, Na+, K+, Rb+, Cs+ was examined by 'H-NMR, FAB mass, and UV spectrometry.

引用

页码：893 / 898

页数：6

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