Beneficial effects of microwave assisted heating versus conventional heating in synthesis of cyclodextrin based nanosponges

被引：15
|
作者：
Singireddy, Anandam [1 ]
Pedireddi, Sobhita Rani [2 ]
Nimmagadda, Srinivas [2 ]
Subramanian, Selvamuthukumar [1 ]
机构：
[1] Annamalai Univ, Fac Engn & Technol, Dept Pharm, Annamalainagar 608002, Tamil Nadu, India
[2] Malla Reddy Pharm Coll, Hyderabad 500100, Andhra Pradesh, India
来源：
MATERIALS TODAY-PROCEEDINGS | 2016年 / 3卷 / 10期
关键词：
Nanosponges; Cyclodextrins; Microwave Synthesis; Crystallinity; Polyd spers ty index; BETA-CYCLODEXTRIN; ORGANIC POLLUTANTS; REMOVAL; WATER;
D O I：
10.1016/j.matpr.2016.11.055
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The effects of microwave heating versus conventional heating on particle-size distribution, morphology and crystallinity of cyclodextrin nanosponges have been investigated. FTIR-ATR, XRPD, DSC and DTA studies outlined the structural differences between the nanosponges prepared by different methods. The microwave synthesized nanosponges exhibited higher degree of crystallinity and narrow size distribution. HR-TEM indicates that nanosponges obtained from microwave method are highly crystalline and faceted versus their conventionally prepared counterparts. Microwave-synthesized nanosponges were measured with approximately twice the loading capacity towards a model drug than similar-sized conventionally prepared particles. Extensive structural characterisation studies revealed the distinct and preferential effects of the microwave heating method. (C) 2016 Elsevier Ltd. All rights reserved.
引用
收藏
页码：3951 / 3959
页数：9
相关论文
共 50 条
  • [21] β-Cyclodextrin Based Nanosponges in Organic Synthesis
    Kiasat, Ali R.
    Saghanezhad, Seyyed J.
    Noori, Samaneh
    CURRENT ORGANIC CHEMISTRY, 2019, 23 (21) : 2366 - 2377
  • [22] Microwave versus Conventional Heating in the Grafting of Alkyltrimethoxysilanes onto Silica Particles
    Garcia, Nuria
    Benito, Esperanza
    Guzman, Julio
    de Francisco, Raquel
    Tiemblo, Pilar
    LANGMUIR, 2010, 26 (08) : 5499 - 5506
  • [23] Microwave and conventional heating effects on thermoxidative degradation of edible fats
    Albi, T
    Lanzon, A
    Guinda, A
    Leon, M
    PerezCamino, MC
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (10) : 3795 - 3798
  • [24] Cooperative Application of Conventional and Microwave Heating
    Fulo, Harvey F.
    Vincent, Morgan A.
    Stiegman, Albert E.
    Dudley, Gregory B.
    ASIAN JOURNAL OF ORGANIC CHEMISTRY, 2020, 9 (06) : 961 - 966
  • [25] Microwave-assisted synthesis of various ZnO hierarchical nanostructures: Effects of heating parameters of microwave oven
    Zhu, Pengli
    Zhang, Jingwei
    Wu, Zhishen
    Zhang, Zhijun
    CRYSTAL GROWTH & DESIGN, 2008, 8 (09) : 3148 - 3153
  • [26] Furfural Synthesis from d-Xylose in the Presence of Sodium Chloride: Microwave versus Conventional Heating
    Xiouras, Christos
    Radacsi, Norbert
    Sturm, Guido
    Stefanidis, Georgios D.
    CHEMSUSCHEM, 2016, 9 (16) : 2159 - 2166
  • [27] Plam oil empty fruit bunch based magnetic biochar composite comparison for synthesis by microwave-assisted and conventional heating
    Mubarak, N. M.
    Sahu, J. N.
    Abdullah, E. C.
    Jayakumar, N. S.
    JOURNAL OF ANALYTICAL AND APPLIED PYROLYSIS, 2016, 120 : 521 - 528
  • [28] Facile Synthesis of Polycrystalline NiO Nanorods Assisted by Microwave Heating
    Song, Xuefeng
    Gao, Lian
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2008, 91 (10) : 3465 - 3468
  • [29] Facile synthesis of polycrystalline NiO nanorods assisted by microwave heating
    Song, Xuefeng
    Gao, Lian
    Journal of the American Ceramic Society, 2008, 91 (10): : 3465 - 3468
  • [30] Synthesis of unsubstituted cyclic imides assisted by microwave heating.
    Hijji, Y
    Menjamin, E
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2002, 223 : B239 - B239
12345