Synthesis and crystal structure of triphenyltin diphenylthiocarbazone

被引：0
|
作者：
Zhang, RF
Li, F
Ma, CL [1 ]
机构：
[1] Liaocheng Univ, Dept Chem, Liaocheng 252059, Peoples R China
[2] Taishan Univ, Tai An 271021, Peoples R China
来源：
INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY | 2004年 / 43卷 / 05期
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D O I：
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中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The compound (Ph3SnSN4C13H11) has been prepared by the reaction of triphenyltin chloride with diphenylthiocarbazone in sodium alcoholic. Its structure has been determined with IR, H-1 NMR and X-ray crystallography. It crystallizes in the monoclinic, space group P-1, a=8.608(2) Angstrom, b=11.991 (3) Angstrom, c=13.760(3) Angstrom, alpha=98.912(3) degrees, beta=94.961(4) degrees, gamma=94.086(4) degrees, Z=2, V=1392.7 (6) Angstrom(3), D-c=1.443 g/cm(3), mu=1.019 mm(-1), F(000)=612, R-1=0.0639, wR(2)=0.0593. The central Sn atom is distorted trigonal bipyramid.
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页码：1109 / 1111
页数：3
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