Determination of tylosin in milk by reversed-phase liquid chromatography

被引：0
|
作者：
Usleber, E [1 ]
Straka, M [1 ]
Martlbauer, E [1 ]
机构：
[1] UNIV MUNICH,FAC VET,INST HYG & TECHNOL FOOD ANIM ORIGIN,D-80539 MUNICH,GERMANY
来源：
ARCHIV FUR LEBENSMITTELHYGIENE | 1997年 / 48卷 / 04期
关键词：
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
A method for the determination of tylosin in milk is reported. Milk samples were defatted, diluted with water and purified using RP18 solid phase extraction columns. Determination was achieved by reversed-phase liquid chromatography and UV detection at 287 nm. Peak identity was checked by recording the UV spectrum. Detection limit for tylosin in milk was 12.5-15 ng/ml. Recoveries for tylosin from spiked milk samples (concentration range: 25-100 ng/ml) were 81.7-87.6%, with coefficients of variation of 7.32-17.1%.
引用
收藏
页码：75 / 76
页数：2
相关论文
共 50 条
  • [31] Determination of lipid profile in meningococcal polysaccharide reversed-phase liquid chromatography
    Li, Y
    Lander, R
    Manger, W
    Lee, A
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2004, 804 (02): : 353 - 358
  • [32] Determination of ramipril in pharmaceutical dosage forms by reversed-phase liquid chromatography
    Rao, KVSP
    Kumari, KV
    Prakash, IB
    Prabhakar, G
    Begum, J
    ASIAN JOURNAL OF CHEMISTRY, 2006, 18 (02) : 788 - 792
  • [33] Determination of Atorvastatin and Gemfibrozil in Human Plasma by Reversed-Phase Liquid Chromatography
    Khan, Islam U.
    Jillani, Shehzada M. S.
    Ashfaq, Muhammad
    LATIN AMERICAN JOURNAL OF PHARMACY, 2010, 29 (08): : 1383 - 1388
  • [34] Determination of tea catechins by reversed-phase high performance liquid chromatography
    Hollman, PCH
    Venema, DP
    Khokhar, S
    Arts, ICW
    OXIDANTS AND ANTIOXIDANTS, PT A, 1999, 299 : 202 - 206
  • [35] DETERMINATION OF NIFEDIPINE IN SERUM OR PLASMA BY REVERSED-PHASE LIQUID-CHROMATOGRAPHY
    BACH, PR
    CLINICAL CHEMISTRY, 1983, 29 (07) : 1344 - 1348
  • [36] DETERMINATION OF DIMETHYL SULFATE IN AIR BY REVERSED-PHASE LIQUID-CHROMATOGRAPHY
    WILLIAMS, RG
    JOURNAL OF CHROMATOGRAPHY, 1982, 245 (03): : 381 - 384
  • [37] DETERMINATION OF MOLYBDENUM AND TUNGSTEN WITH TIRON BY REVERSED-PHASE LIQUID-CHROMATOGRAPHY
    YAMADA, H
    HATTORI, T
    JOURNAL OF CHROMATOGRAPHY, 1985, 320 (02): : 403 - 407
  • [38] DETERMINATION OF FLUVOXAMINE CONCENTRATION IN PLASMA BY REVERSED-PHASE LIQUID-CHROMATOGRAPHY
    WONG, SHY
    KRANZLER, HR
    DELLAFERA, S
    FERNANDES, R
    BIOMEDICAL CHROMATOGRAPHY, 1994, 8 (06) : 278 - 282
  • [39] Amphotericin B determination in respiratory secretions by reversed-phase liquid chromatography
    Lopez, R
    Pou, L
    Andres, I
    Monforte, V
    Roman, A
    Pascual, C
    JOURNAL OF CHROMATOGRAPHY A, 1998, 812 (1-2) : 135 - 139
  • [40] Comparison of micellar and reversed-phase liquid chromatography for determination of sulfamethoxazole and trimethoprim
    Kulikov, AU
    Verushkin, AG
    Loginova, LP
    CHROMATOGRAPHIA, 2005, 61 (9-10) : 455 - 463
12345