Characterization of pure and doped potassium hydrogen tartrate single crystals grown in silica gel

被引：18

作者：

Quasim, I. ^{[1
]}

Firdous, A. ^{[2
]}

Sahni, N. ^{[3
]}

Khosa, S. K. ^{[1
]}

Kotru, P. N. ^{[1
]}

机构：

[1] Univ Jammu, Dept Phys & Elect, Crystal Growth & Mat Res Lab, Jammu 180006, India

[2] Natl Inst Technol, Dept Phys, Kashmir 190006, Jammu & Kashmir, India

[3] Panjab Univ, Dept Geol, Chandigarh 160014, India

来源：

CRYSTAL RESEARCH AND TECHNOLOGY | 2009年 / 44卷 / 05期

关键词：

gel technique; doped potassium hydrogen tartrate; SEM; XRD; CH analysis; FTIR spectroscopy; TGA;

D O I：

10.1002/crat.200800617

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Growth of pure-, sodium- and lithium- doped potassium hydrogen tartrate single crystals by gel technique is reported. Growth conditions conducive for the growth of single crystals are worked out. The crystals are characterized by using powder XRD, SEM, FTIR, AES, EDAX, CH analysis and thermoanalytical techniques. The stoichiometric composition for the grown crystals are established as KHC4H4O6 center dot H2O, (K)(0.98)(Na)(0.02)HC4H4O6 center dot H2O and (K)(0.94)(Li)(0.06)HC4H4O6 center dot H2O. Doping of sodium and lithium in the pure potassium hydrogen tartrate single crystals is found to influence the size, perfection, morphology, crystal structure and the thermal stability of crystals. (C) 2009 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

引用

页码：539 / 547

页数：9

共 50 条

[1] Micromechanical behaviour of gel grown pure and doped potassium hydrogen tartrate single crystals
Quasim, I.
Firdous, A.
Sahni, N.
Khosa, S. K.
Kotru, P. N.
PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE, 2009, 206 (12): : 2791 - 2800
[2] Characterization of pure and copper-doped iron tartrate crystals grown in silica gel
Mathivanan, V.
Haris, M.
PRAMANA-JOURNAL OF PHYSICS, 2013, 81 (01): : 177 - 187
[3] Characterization of pure and copper-doped iron tartrate crystals grown in silica gel
V MATHIVANAN
M HARIS
Pramana, 2013, 81 : 177 - 187
[4] Growth and characterization of gel grown potassium hydrogen levo-tartrate crystals
Govani, Jayesh
Joshi, Mihir J.
INDIAN JOURNAL OF PHYSICS, 2008, 82 (11) : 1485 - 1494
[5] Optical and electrical characteristics of pure and doped potassium hydrogen tartrate single crystals
Quasim, I.
Firdous, A.
Khosa, S. K.
Kotru, P. N.
JOURNAL OF PHYSICS D-APPLIED PHYSICS, 2009, 42 (15)
[6] A comparative study of pure and potassium doped cadmium mercury thiocyanate single crystals grown in silica gel
Kumari, P. Nisha Santha
Margaret, M. Beatrice
Kalainathan, S.
CRYSTAL RESEARCH AND TECHNOLOGY, 2009, 44 (02) : 177 - 183
[7] Growth of doped potassium perchlorate single crystals in silica gel and their characterization
Ramamurthi, K
Kaliannan, P
Ganesamurthy, K
Kathalingam, A
CRYSTAL RESEARCH AND TECHNOLOGY, 1998, 33 (02) : 177 - 181
[8] GROWTH AND CHARACTERIZATION OF PURE AND DOPED LEAD HYDROGEN PHOSPHATE SINGLE-CRYSTALS IN SILICA-GEL
MANIMEKALAI, R
BALAKRISHNAN, T
RAMAMURTHI, K
CRYSTAL RESEARCH AND TECHNOLOGY, 1994, 29 (06) : 795 - 800
[9] Studies on solution-grown pure and doped Sodium Potassium tartrate crystals
Mathivanan, V.
Haris, M.
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2013, 102 : 341 - 349
[10] Characterization, microhardness and dielectric studies of pure and doped (copper, cadmium) barium oxalate single crystals grown in silica gel
Salim, M. Abdul
Raveendran, R.
ASIAN JOURNAL OF CHEMISTRY, 2008, 20 (08) : 5971 - 5976

← 1 2 3 4 5 →