Synthesis and characterization of dialkyldithiophosphate complexes of gallium(III)

被引：0

作者：

Pahari, D ^{[1
]}

Jain, VK ^{[1
]}

机构：

[1] BHABHA ATOM RES CTR,DIV CHEM,BOMBAY 400085,MAHARASHTRA,INDIA

来源：

MAIN GROUP METAL CHEMISTRY | 1997年 / 20卷 / 11期

关键词：

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Treatment of gallium(III) chloride with ammonium dialkyldithiophosphate in benzene afford complexes of the type [GaCl3.n{S2P(OR)(2)}(n)] (n = 1,2,3; R = Et, Pr-n, Pr-i). The chloro complexes can be readily obtained by the reaction of gallium trichloride with gallium tris(dialkyldithiophosphate) in benzene at room temperature. All these complexes were characterized by elemental analysis, IR, NMR (H-1, C-13 and P-31) and spectral data. NMR studies indicate the monochloro complexes to be fluxional at room temperature.

引用

页码：691 / 696

页数：6

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