Mn3O4@ZnO Core-Shell Nanocomposite: Synthesis and Characterization

被引：4
|
作者：
Shafiu, S. [1 ,2 ]
Kavas, H. [3 ]
Baykal, A. [1 ]
机构：
[1] Fatih Univ, Dept Chem, TR-34500 Istanbul, Turkey
[2] Kano Univ Sci & Technol, Kano, Nigeria
[3] Istanbul Medeniyet Univ, Dept Phys, TR-34700 Istanbul, Turkey
来源：
JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2014年 / 24卷 / 03期
关键词：
Mn3O4; Zinc oxide; Core-shell structures; Nanocomposite; Magnetization; MAGNETIC-PROPERTIES; MN3O4; NANOPARTICLES; ZINC-OXIDE; PHOTOLUMINESCENCE; NANOCRYSTALS; TEMPERATURE; OXIDATION; MNO;
D O I：
10.1007/s10904-013-0014-8
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Nano-sized single-phase Mn3O4@ZnO core-shell nanocomposite was prepared via a simple one-pot sequential polyol using triethylene glycol as a high boiling point solvent as well as a reducing agent. The presence of both Mn3O4 and ZnO was confirmed with X-ray diffractometry. Infrared measurements proved the presence of triethylene glycol on the surface of Mn3O4@ZnO core-shell. The average particle size is between 8 and 13 nm. Reference intensity ratios method calculations showed that the weight percentage of phases were found as 54.7 % ZnO and 45.3 % Mn3O4. The lower Tc maybe explained by interface effects and dominant ZnO shell in magnetic properties of core-shell nanocomposite.
引用
收藏
页码：531 / 535
页数：5
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