Mn3O4@ZnO Core-Shell Nanocomposite: Synthesis and Characterization

被引：4
|
作者：
Shafiu, S. [1 ,2 ]
Kavas, H. [3 ]
Baykal, A. [1 ]
机构：
[1] Fatih Univ, Dept Chem, TR-34500 Istanbul, Turkey
[2] Kano Univ Sci & Technol, Kano, Nigeria
[3] Istanbul Medeniyet Univ, Dept Phys, TR-34700 Istanbul, Turkey
来源：
JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2014年 / 24卷 / 03期
关键词：
Mn3O4; Zinc oxide; Core-shell structures; Nanocomposite; Magnetization; MAGNETIC-PROPERTIES; MN3O4; NANOPARTICLES; ZINC-OXIDE; PHOTOLUMINESCENCE; NANOCRYSTALS; TEMPERATURE; OXIDATION; MNO;
D O I：
10.1007/s10904-013-0014-8
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Nano-sized single-phase Mn3O4@ZnO core-shell nanocomposite was prepared via a simple one-pot sequential polyol using triethylene glycol as a high boiling point solvent as well as a reducing agent. The presence of both Mn3O4 and ZnO was confirmed with X-ray diffractometry. Infrared measurements proved the presence of triethylene glycol on the surface of Mn3O4@ZnO core-shell. The average particle size is between 8 and 13 nm. Reference intensity ratios method calculations showed that the weight percentage of phases were found as 54.7 % ZnO and 45.3 % Mn3O4. The lower Tc maybe explained by interface effects and dominant ZnO shell in magnetic properties of core-shell nanocomposite.
引用
收藏
页码：531 / 535
页数：5
相关论文
共 50 条
  • [1] Mn3O4@ZnO Core–Shell Nanocomposite: Synthesis and Characterization
    S. Shafiu
    H. Kavas
    A. Baykal
    [J]. Journal of Inorganic and Organometallic Polymers and Materials, 2014, 24 : 531 - 535
  • [2] Controlled Synthesis of Core-shell Structured Mn3O4@ZnO Nanosheet Arrays for Aqueous Zinc-ion Batteries
    Li Meng-Xia
    Lu Yue
    Wang Li-Bin
    Hu Xian-Luo
    [J]. JOURNAL OF INORGANIC MATERIALS, 2020, 35 (01) : 86 - 92
  • [3] Synthesis and Characterization of Fe3O4 @ Polyrhodanine Nanocomposite with Core-Shell Morphology
    Rahmanzadeh, Lida
    Ghorbani, Mohsen
    Jahanshahi, Mohsen
    [J]. ADVANCES IN POLYMER TECHNOLOGY, 2014, 33
  • [4] Synthesis and characterization of Fe3O4@ZnO core-shell structured nanoparticles
    Wan, Jiaqi
    Li, Hui
    Chen, Kezheng
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2009, 114 (01) : 30 - 32
  • [5] Synthesis and Characterization of Ferromagnetic Fe3O4-ZnO Hybrid Core-Shell Nanoparticles
    Nishad, K. K.
    Tiwari, Neha
    Pandey, R. K.
    [J]. JOURNAL OF ELECTRONIC MATERIALS, 2018, 47 (07) : 3440 - 3450
  • [6] Hydrothermal Synthesis of Core/Shell ZnO:Mn/Mn3O4 Nanowires
    Eastman, Micah
    Besser, Aaron
    Chen, Yanxue
    Jiao, Jun
    [J]. JOURNAL OF PHYSICAL CHEMISTRY C, 2011, 115 (22): : 10979 - 10984
  • [7] Bifunctional core-shell nanocomposite Mn-doped ZnO/Fe3O4 for photodegradation of reactive blue 198 dye
    Nguyen, Van Cuong
    [J]. ADVANCES IN NATURAL SCIENCES-NANOSCIENCE AND NANOTECHNOLOGY, 2014, 5 (03)
  • [8] Photocatalytic Degradation Process of Bisacodyl Using Fe3O4@ZnO Core-Shell Nanocomposite
    Mahboob, Amin Dadras
    Khoshnood, Razieh Sanavi
    [J]. RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY A, 2022, 96 (14) : 3274 - 3282
  • [9] Photocatalytic Degradation Process of Bisacodyl Using Fe3O4@ZnO Core-Shell Nanocomposite
    Razieh Sanavi Amin Dadras Mahboob
    [J]. Russian Journal of Physical Chemistry A, 2022, 96 : 3274 - 3282
  • [10] A novel magnetic core-shell nanocomposite Fe3O4@chitosan@ZnO for the green synthesis of 2-benzimidazoles
    Fei Tian
    Libo Niu
    Bo Chen
    Xuejia Gao
    Xingwang Lan
    Li Huo
    Guoyi Bai
    [J]. Journal of Nanoparticle Research, 2017, 19
12345