Visualizing polymeric liquid/solid interfaces by atomic force microscopy utilizing quartz tuning fork sensors

被引:10
|
作者
Yamada, Yuya [1 ]
Ichii, Takashi [1 ]
Utsunomiya, Toru [1 ]
Sugimura, Hiroyuki [1 ]
机构
[1] Kyoto Univ, Grad Sch Engn, Dept Mat Sci & Engn, Kyoto 6068501, Japan
关键词
VISCOELASTIC PROPERTIES; SHEAR ELASTICITY; SOLID-SURFACES; FILMS; FRICTION; LUBRICATION;
D O I
10.35848/1347-4065/ab84b0
中图分类号
O59 [应用物理学];
学科分类号
摘要
We investigated a polymeric liquid/solid interface by frequency modulation atomic force microscopy (FM-AFM) using a quartz tuning fork sensor, so-called qPlus sensor. We carried out topographic imaging on a muscovite mica surface in poly(dimethylsiloxane) (PDMS) which has 1000 times higher viscosity than that of water and the crystal structure of the mica surface was successfully imaged. Two-dimensional frequency shift mapping was also demonstrated at the interface and the layered structure of density distribution of the PDMS was imaged. The monotonic energy dissipation curve indicated the fluid-like behavior of the PDMS near the mica surface. In addition, lateral variation of density distribution was also imaged. The results in this work indicated usefulness of FM-AFM using qPlus sensors for lubrication study. (C) 2020 The Japan Society of Applied Physics
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页数:5
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