Upgrade of a Raman spectrometer

被引:6
|
作者
Hansen, SB [1 ]
Berg, RW
StenbY, EH
机构
[1] Tech Univ Denmark, Dept Chem Engn, DK-2800 Lyngby, Denmark
[2] Tech Univ Denmark, Engn Res Ctr, Dept Chem Engn, IVC,SEP, DK-2800 Lyngby, Denmark
关键词
instrumentation; Raman spectroscopy; CCD detector; calibration;
D O I
10.1081/ASR-200030198
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
improvement of a conventional JEOL Raman spectrometer with a single channel photo multiplier detector is described. New optical components [fibers, mirror, lens, and charge coupled device detector (CCD)] have been chosen to design a high quality and easy-to-use instrument. Tests have shown that with this modified spectrometer, Raman spectra can be acquired of a quality comparable to the spectra obtained previously, but the time needed to obtain a spectrum is markedly reduced. Selected test spectra and a simple calibration procedure to obtain the wavenumber values from the band CCD pixel position are presented.
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页码:385 / 397
页数:13
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