Mossbauer investigation of γ-Fe2O3 nanocrystals in silica matrix prepared by the sol-gel method

被引:0
|
作者
Cannas, C
Concas, G
Congiu, F
Musinu, A
Piccaluga, G
Spano, G
机构
[1] Univ Cagliari, Dipartimento Fis, I-09042 Cagliari, Italy
[2] INFM, I-09042 Cagliari, Italy
[3] Univ Cagliari, Dipartimento Sci Chim, I-09042 Cagliari, Italy
关键词
nanostructures; oxides; sol-gel growth; Mossbauer spectroscopy; magnetic properties;
D O I
暂无
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A series of Fe2O3-SiO2 nnocomposites (25 weight % of Fe2O3) has been prepared using a sol-gel method, Samples showing different features were obtained by varying the evaporation conditions acting on the surface / volume ratio of the starting sol. The samples were investigated using Mossbauer spectroscopy at low temperature. The Fe2O3 nanoparticles have been identified as maghemite (gamma-Fe2O3) particles. The samples show a superparamagnetic behavior with a blocking temperature that depends on the average particle size.
引用
收藏
页码:154 / 158
页数:5
相关论文
共 50 条
  • [41] Effect of Drying Conditions on the Characteristics and Performance of B/Fe2O3 Nano-Composites Prepared by Sol-Gel Method
    Yilmaz, Nil Ezgi Dincer
    Karakas, Gurkan
    CENTRAL EUROPEAN JOURNAL OF ENERGETIC MATERIALS, 2020, 17 (01): : 85 - 106
  • [42] Photocatalytic degradation of methylene blue dye using Fe2O3/TiO2 nanoparticles prepared by sol-gel method
    Ahmed, M. A.
    El-Katori, Emad E.
    Gharni, Zarha H.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2013, 553 : 19 - 29
  • [43] Nanocomposites Fe2O3/SiO2-preparation by sol-gel method and physical properties
    D. Niznansky
    N. Viart
    J. L. Rehspringer
    Journal of Sol-Gel Science and Technology, 1997, 8 : 615 - 618
  • [44] Nanocomposites Fe2O3/SiO2-preparation by sol-gel method and physical properties
    Niznansky, D
    Viart, N
    Rehspringer, JL
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 1997, 8 (1-3) : 615 - 618
  • [45] Preparation of γ-Fe2O3 Doped with Co2+ and Dy3+ by Sol-Gel Method
    Zhu, Lizhong
    Shi, Haowei
    Yang, Huan
    Yang, Yuxiang
    Yuan, Hongming
    Xie, Xiaocui
    Liu, Xiangnong
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2017, 17 (06) : 4372 - 4383
  • [46] Nanocomposites Fe2O3/SiO2-Preparation by Sol-Gel Method and Physical Properties
    D. Niznansky
    N. Viart
    J.L. Rehspringer
    Journal of Sol-Gel Science and Technology, 1997, 8 : 615 - 618
  • [47] Characterization and evaluation of Fe2O3/Al2O3 oxygen carrier prepared by sol-gel combustion synthesis
    Wang, Baowen
    Yan, Rong
    Lee, Dong Ho
    Zheng, Ying
    Zhao, Haibo
    Zheng, Chuguang
    JOURNAL OF ANALYTICAL AND APPLIED PYROLYSIS, 2011, 91 (01) : 105 - 113
  • [48] Photoelectrochemical Properties of Fe2O3-SnO2 Films Prepared by Sol-Gel Method
    Uchiyama, Hiroaki
    Yukizawa, Masashi
    Kozuka, Hiromitsu
    JOURNAL OF PHYSICAL CHEMISTRY C, 2011, 115 (14): : 7050 - 7055
  • [49] Size and shape controlled of α-Fe2O3 nanoparticles prepared via sol-gel technique and their photocatalytic activity
    Ba-Abbad, Muneer M.
    Takriff, Mohd S.
    Benamor, Abdelbaki
    Mohammad, Abdul Wahab
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2017, 81 (03) : 880 - 893
  • [50] Sol-gel synthesis of α-Fe2O3 nanoparticles and its photocatalytic application
    Alagiri, M.
    Hamid, Sharifah Bee Abdul
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2015, 74 (03) : 783 - 789