Nano-sized zirconium carbide powder: Synthesis and densification using a spark plasma sintering apparatus

被引：26
|
作者：
Feng, Lun [1 ]
Lee, Seahoon [1 ]
Lee, Heesoo [2 ]
机构：
[1] Korea Inst Mat Sci, Div Powder, Div Ceram Res, Chang Won 641831, South Korea
[2] Pusan Natl Univ, Sch Mat Sci & Engn, Busan 609735, South Korea
来源：
INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS | 2017年 / 64卷
关键词：
Zirconium carbide; Nanoparticles; Synthesis; Spark plasma sintering; Densification; HAFNIUM;
D O I：
10.1016/j.ijrmhm.2017.01.006
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Nano-sized zirconium carbide powder was synthesized at 1600 degrees C by the carbothermal reduction of ZrO2 using a modified spark plasma sintering (SPS) apparatus. The synthesized ZrC powder had a fine particle size of approximately 189 nm and a low oxygen content of 0.88 wt%. The metal basis purity of the synthesized powder was 99.87%. The low synthesis temperature, fast heating/cooling rate and the effect of current during the modified SPS process effectively suppressed the particle growth. Using the synthesized powder, monolithic ZrC ceramics with high relative density (97.14%) were obtained after the densification at 2100 degrees C for 30 min at a pressure of 80 MPa by SPS. The average grain size of the densified ZrC ceramics was approximately 9.12 mu m. (C) 2017 Elsevier Ltd. All rights reserved.
引用
收藏
页码：98 / 105
页数：8
相关论文
共 50 条
  • [21] Synthesis and Characterization of Nano-sized Boron Powder Prepared by Plasma Torch
    黄志军
    吴青友
    李祥
    尚书勇
    戴晓雁
    印永祥
    Plasma Science and Technology, 2010, (05) : 577 - 580
  • [22] Synthesis and Characterization of Nano-sized Boron Powder Prepared by Plasma Torch
    Huang Zhijun
    Wu Qingyou
    Li Xiang
    Shang Shuyong
    Dai Xiaoyan
    Yin Yongxiang
    PLASMA SCIENCE & TECHNOLOGY, 2010, 12 (05) : 577 - 580
  • [23] Synthesis and Characterization of Nano-sized Boron Powder Prepared by Plasma Torch
    黄志军
    吴青友
    李祥
    尚书勇
    戴晓雁
    印永祥
    Plasma Science and Technology, 2010, 12 (05) : 577 - 580
  • [24] Densification behaviour of pure molybdenum powder by spark plasma sintering
    Ohser-Wiedemann, R.
    Martin, U.
    Seifert, H. J.
    Mueller, A.
    INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS, 2010, 28 (04): : 550 - 557
  • [25] Densification and grain growth kinetics of boron carbide powder during ultrahigh temperature spark plasma sintering
    Zhang, Mei
    Wang, Wen-jun
    Yuan, Tie-chui
    Xie, Si-yao
    Li, Rui-di
    Zhou, Zhi-hui
    Xu, Yun-bao
    TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA, 2022, 32 (06) : 1948 - 1960
  • [26] Spark plasma sintering of fine uranium carbide powder
    Salvato, D.
    Vigier, J. -F.
    Cologna, M.
    Luzzi, L.
    Somers, J.
    Tyrpekl, V.
    CERAMICS INTERNATIONAL, 2017, 43 (01) : 866 - 869
  • [27] Densification and grain growth kinetics of boron carbide powder during ultrahigh temperature spark plasma sintering
    ZHANG, Mei
    WANG, Wen-jun
    YUAN, Tie-chui
    XIE, Si-yao
    LI, Rui-di
    ZHOU, Zhi-hui
    XU, Yun-bao
    Transactions of Nonferrous Metals Society of China (English Edition), 2022, 32 (06): : 1948 - 1960
  • [28] Spark plasma sintering of agglomerated vanadium carbide powder
    Li, Wei
    Olevsky, Eugene A.
    Khasanov, Oleg L.
    Back, Christina A.
    Izhvanov, Oleg
    Opperman, Jonas
    Khalifa, Hesham E.
    CERAMICS INTERNATIONAL, 2015, 41 (03) : 3748 - 3759
  • [29] Zirconium Carbide Produced by Spark Plasma Sintering and Hot Pressing: Densification Kinetics, Grain Growth, and Thermal Properties
    Wei, Xialu
    Back, Christina
    Izhvanov, Oleg
    Haines, Christopher D.
    Olevsky, Eugene A.
    MATERIALS, 2016, 9 (07)
  • [30] Microwave-plasma synthesis of nano-sized silicon carbide at atmospheric pressure
    van Laar, J. H.
    Slabber, J. F. M.
    Meyer, J. P.
    van der Walt, I. J.
    Puts, G. J.
    Crouse, P. L.
    CERAMICS INTERNATIONAL, 2015, 41 (03) : 4326 - 4333
12345