The synthesis, structure, and properties of carbon-containing nanocomposites based on nickel, palladium, and iron

被引：21
|
作者：
Ermakov, A. E. [1 ]
Uimin, M. A. [1 ]
Lokteva, E. S. [2 ]
Mysik, A. A. [1 ]
Kachevskii, S. A. [2 ]
Turakulova, A. O. [2 ]
Gaviko, V. S. [1 ]
Lunin, V. V. [2 ]
机构：
[1] Russian Acad Sci, Inst Met Phys, Ural Div, Ekaterinburg 620219, Russia
[2] Moscow MV Lomonosov State Univ, Fac Chem, Moscow, Russia
来源：
RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY A | 2009年 / 83卷 / 07期
基金：
俄罗斯基础研究基金会;
关键词：
ARC-DISCHARGE; ENCAPSULATED NANOPARTICLES; NANOCAPSULES; PARTICLES; NANOTUBES; ALLOYS; NI;
D O I：
10.1134/S0036024409070243
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Nickel, iron, palladium, and bimetallic nickel-palladium nanoparticles encapsulated in carbon were synthesized by contactless levitation fusion of metals in a magnetic field in a flow of an inert gas containing a hydrocarbon. The products were characterized by X-ray diffraction, differential thermal analysis, thermogravimetry, high-resolution transmission electron microscopy, and adsorption. A layered carbon shell preventing agglomeration and oxidation formed on the surface of nickel- and iron-containing particles. The size of particles depended on preparation conditions and could be of 5-15 nm.
引用
收藏
页码：1187 / 1193
页数：7
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