Five-membered 2,3-dioxo heterocycles: LXVI. Reactions of (2Z,5Z)-1-aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones with o-phenylenediamine and hydrazine. Crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone

被引：3

作者：

Khalturina, V. V. ^{[1
]}

Shklyaev, Yu. V. ^{[1
]}

Aliev, Z. G. ^{[2
]}

Maslivets, A. N. ^{[3
]}

机构：

[1] Russian Acad Sci, Inst Tech Chem, Ural Div, Perm, Russia

[2] Russian Acad Sci, Inst Chem Phys Problems, Chernogolovka, Moscow Oblast, Russia

[3] Perm State Univ, Perm 614990, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2009年 / 45卷 / 10期

基金：

俄罗斯基础研究基金会;

关键词：

1,3,4,6-TETRACARBONYL COMPOUNDS;

D O I：

10.1134/S1070428009100169

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

(2Z,5Z)-1-Aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones reacted with o-phenylenediamine and hydrazine to give 3-[(Z)-2-aryl-2-oxoethylidene]-1,2,3,4-tetrahydroquinoxalin-2-ones and 1-(3-aryl-1H-pyrazol-5-yl)-2-[(Z)-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]ethanones, respectively. The crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone was determined by X-ray analysis.

引用

页码：1519 / 1522

页数：4

共 46 条

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Kempe, R
Spannenberg, A
Heller, D
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1998, 213 (03): : 633 - 635
[42] Five-membered 2,3-dioxo heterocycles:: LXI.: Reaction of 3-aroyl-1H-pyrrolo[2,1-c][1,4]benzoxazine-1,2,4-triones with α-enamino esters.: Crystalline and molecular structure of methyl 11-benzoyl-2-o-hydroxyphenyl-3,4,10-trioxo-6,9-diphenyl-7-oxa-2,9-diazatricyclo[6.2.1.01,5]undec-5-ene-8-carboxylate
Racheva, N. L.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 44 (08) : 1184 - 1188
[43] Five-membered 2,3-dioxo heterocycles: LXXXIX. Reaction of methyl 1-aryl-3-cinnamoyl-4,5-dioxo-4,5-dihydro-1H-pyrrole-2-carboxylates with (E)-4-arylaminopent-3-en-2-ones. Crystalline and molecular structure of 9-acetyl-4-cinnamoyl-3-hydroxy-1-(4-methoxyphenyl)-8-methyl-7-phenyl-1,7-diazaspiro[4.4]nona-3,8-diene-2,6-dione
P. S. Silaichev
V. O. Filimonov
P. A. Slepukhin
A. N. Maslivets
Russian Journal of Organic Chemistry, 2012, 48 : 1329 - 1332
[44] Five-membered 2,3-dioxo heterocycles: LXI. Reaction of 3-aroyl-1H-pyrrolo[2,1-c][1,4]benzoxazine-1,2,4-triones with α-enamino esters. Crystalline and molecular structure of methyl 11-benzoyl-2-o-hydroxyphenyl-3,4,10-trioxo-6,9-diphenyl-7-oxa-2,9-diazatricyclo[6.2.1.01,5]undec-5-ene-8-carboxylate
N. L. Racheva
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2008, 44 : 1184 - 1188
[45] Five-membered 2,3-dioxo heterocycles: LXXXIX. Reaction of methyl 1-aryl-3-cinnamoyl-4,5-dioxo-4,5-dihydro-1H-pyrrole-2-carboxylates with (E)-4-arylaminopent-3-en-2-ones. Crystalline and molecular structure of 9-acetyl-4-cinnamoyl-3-hydroxy-1-(4-methoxyphenyl)-8-methyl-7-phenyl-1,7-diazaspiro[4.4]nona-3,8-diene-2,6-dione
Silaichev, P. S.
Filimonov, V. O.
Slepukhin, P. A.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2012, 48 (10) : 1329 - 1332
[46] Crystal structure of (Z)-N-(17-(1-(dimethylamino)ethyl)-10,13-dimethyl-4-oxo-4,5,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta-[a]phenanthren-3-yl)-3-methylbut-2-enimidic acid dichloromethane monosolvate, C29H45Cl2N2O2
He, Kang
Zou, Juan
Wang, Jin Xi
Du, Jiang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2013, 228 (03): : 327 - 328

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