Five-membered 2,3-dioxo heterocycles: LXVI. Reactions of (2Z,5Z)-1-aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones with o-phenylenediamine and hydrazine. Crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone

被引：3

作者：

Khalturina, V. V. ^{[1
]}

Shklyaev, Yu. V. ^{[1
]}

Aliev, Z. G. ^{[2
]}

Maslivets, A. N. ^{[3
]}

机构：

[1] Russian Acad Sci, Inst Tech Chem, Ural Div, Perm, Russia

[2] Russian Acad Sci, Inst Chem Phys Problems, Chernogolovka, Moscow Oblast, Russia

[3] Perm State Univ, Perm 614990, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2009年 / 45卷 / 10期

基金：

俄罗斯基础研究基金会;

关键词：

1,3,4,6-TETRACARBONYL COMPOUNDS;

D O I：

10.1134/S1070428009100169

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

(2Z,5Z)-1-Aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones reacted with o-phenylenediamine and hydrazine to give 3-[(Z)-2-aryl-2-oxoethylidene]-1,2,3,4-tetrahydroquinoxalin-2-ones and 1-(3-aryl-1H-pyrazol-5-yl)-2-[(Z)-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]ethanones, respectively. The crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone was determined by X-ray analysis.

引用

页码：1519 / 1522

页数：4

共 46 条

[1] Five-membered 2,3-dioxo heterocycles: LXVI. Reactions of (2Z,5Z)-1-aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones with o-phenylenediamine and hydrazine. Crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 1519 - 1522
[2] Five-membered 2,3-dioxoheterocycles: LXIV. Reactions of 1-methyl-3,4-dihydroisoquinolines with 5-arylfuran-2,3-diones and (Z)-alkyl 4-aryl-2-hydroxy-4-oxobut-2-enoates. Crystal and molecular structure of (2Z,5Z)-3-hydroxy-5-{8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-phenylpent-2-ene-1,4-dione
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 728 - 734
[3] Five-membered 2,3-dioxoheterocycles: LXIV. Reactions of 1-methyl-3,4-dihydroisoquinolines with 5-arylfuran-2,3-diones and (Z)-alkyl 4-aryl-2-hydroxy-4-oxobut-2-enoates. Crystal and molecular structure of (2Z,5Z)-3-hydroxy-5-{8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-phenylpent-2-ene-1,4-dione
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (05) : 728 - 734
[4] Five-membered 2,3-dioxo heterocycles: LXIX. Direct heterocyclization of [3,4-dihydroisoquinolin-1(2H)-ylidene]-acetamides with 5-arylfuran-2,3-diones. Crystalline and molecular structure of (3E,5Z)-3-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-5-(2-oxo-2-phenylethylidene)pyrrolidine-2,4-dione
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (04) : 539 - 542
[5] Five-membered 2,3-dioxo heterocycles: LXIX. Direct heterocyclization of [3,4-dihydroisoquinolin-1(2H)-ylidene]-acetamides with 5-arylfuran-2,3-diones. Crystalline and molecular structure of (3E,5Z)-3-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-5-(2-oxo-2-phenylethylidene)pyrrolidine-2,4-dione
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2010, 46 : 539 - 542
[6] SYNTHESIS AND ANALGESIC AND ANTI-INFLAMMATORY ACTIVITIES OF (2Z, 5Z)-1-ARYL-3-HYDROXY-5-(3,3-DIALKYL-3,4-DIHYDROISOQUINOLIN-1(2H)-YLIDEN)PENT-2-EN-1,4-DIONES
Khalturina, V. V.
Shklyaev, Yu. V.
Makhmudov, R. R.
Maslivets, A. N.
PHARMACEUTICAL CHEMISTRY JOURNAL, 2011, 44 (11) : 594 - 596
[7] Synthesis and analgesic and anti-inflammatory activities of (2Z,5Z)-1-aryl-3-hydroxy-5-(3,3-dialkyl-3,4-dihydroisoquinolin-1(2H)-yliden)pent-2-en-1,4-diones
V. V. Khalturina
Yu. V. Shklyaev
R. R. Makhmudov
A. N. Maslivets
Pharmaceutical Chemistry Journal, 2011, 44 : 594 - 596
[8] Five-membered 2,3-dioxo heterocycles: LXV. Reaction of 1-methyl-3,4-dihydroisoquinolines with aroylketenes. crystalline and molecular structure of (1Z,3Z)-4-hydroxy-1-[6,7-dimethoxy-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-4-phenylbut-3-en-2-one
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (10) : 1515 - 1518
[9] Five-membered 2,3-dioxo heterocycles: LXV. Reaction of 1-methyl-3,4-dihydroisoquinolines with aroylketenes. crystalline and molecular structure of (1Z,3Z)-4-hydroxy-1-[6,7-dimethoxy-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-4-phenylbut-3-en-2-one
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 1515 - 1518
[10] Five-membered 2,3-dioxo heterocycles: CVI. Acylation of substituted (Z)-2-[1,3,4,4a,5,10b-Hexahydrophenanthridin-6(2H)-ylidene]acetamide with aroylketenes. crystal and molecular structure of substituted N-{(Z)-2-[1,3,4,4a,5,10b-Hexahydrophenanthridin-6(2H)-ylidene]acetyl}acrylamide
V. V. Konovalova
Yu. V. Shklyaev
P. A. Slepukhin
A. N. Maslivets
Russian Journal of Organic Chemistry, 2014, 50 : 1357 - 1360

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