I18-the microfocus spectroscopy beamline at the Diamond Light Source

被引:133
|
作者
Mosselmans, J. Frederick W. [1 ]
Quinn, Paul D. [1 ]
Dent, Andrew J. [1 ]
Cavill, Stuart A. [1 ]
Moreno, Sofia Diaz [1 ]
Peach, Andrew [1 ]
Leicester, Peter J. [1 ]
Keylock, Stephen J. [1 ]
Gregory, Simon R. [2 ]
Atkinson, Kirk D. [1 ]
Rosell, Josep Roque [1 ]
机构
[1] Diamond Light Source Ltd, Didcot OX11 0DE, Oxon, England
[2] STFC Daresbury Lab, Warrington WA4 4AD, Cheshire, England
关键词
microfocus; EXAFS; Diamond; XANES; X-ray fluorescence; ELECTROCHEMICAL DEPOSITION; ABSORPTION-SPECTROSCOPY; RAY; TEMPLATES; PLATINUM; MIRRORS; TOOL;
D O I
10.1107/S0909049509032282
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The design and performance of the microfocus spectroscopy beamline at the Diamond Light Source are described. The beamline is based on a 27 mm-period undulator to give an operable energy range between 2 and 20.7 keV, enabling it to cover the K-edges of the elements from P to Mo and the L(3)-edges from Sr to Pu. Micro-X-ray fluorescence, micro-EXAFS and micro-X-ray diffraction have all been achieved on the beamline with a spot size of similar to 3 mu m. The principal optical elements of the beamline consist of a toroid mirror, a liquid-nitrogen-cooled double-crystal monochromator and a pair of bimorph Kirkpatrick-Baez mirrors. The performance of the optics is compared with theoretical values and a few of the early experimental results are summarized.
引用
收藏
页码:818 / 824
页数:7
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