The estimation of pig bone age for forensic application using thermogravimetric analysis

被引:16
|
作者
Raja, S. [1 ,2 ]
Thomas, P. S. [2 ]
Stuart, B. H. [1 ,2 ]
Guerbois, J. P. [2 ]
O'Brien, C. [3 ]
机构
[1] Univ Technol Sydney, Ctr Forens Sci, Sydney, NSW 2007, Australia
[2] Univ Technol Sydney, Dept Chem & Forens Sci, Sydney, NSW 2007, Australia
[3] Univ Ontario, Inst Technol, Fac Sci, Oshawa, ON L1H 7K4, Canada
关键词
Bone; Decomposition; Forensic; Thermogravimetric analysis; X-RAY-DIFFRACTION; THERMAL-DECOMPOSITION; SPECTROSCOPY;
D O I
10.1007/s10973-009-0124-2
中图分类号
O414.1 [热力学];
学科分类号
摘要
An accurate means of determining bone age is a goal for forensic scientists. In this study, thermogravimetric analysis (TGA) has been used to examine pig bone specimens of different post-mortem age. Analysis of bone in both air and nitrogen atmospheres reveals a decrease in total mass loss as the bones age. Two mass loss steps due to the decomposition of the organic bone components were observed and show decreasing trends with age for decomposition in an air atmosphere. In a nitrogen atmosphere the decomposition was observed to be more complex and age dependence of the mass loss for each step was not identified. The TGA data, however, demonstrates the potential of the technique as a means of estimating post-mortem age of forensic bone specimens.
引用
收藏
页码:173 / 176
页数:4
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