Efficient synthesis of chiral acetylene dithioethers in enantiomerically pure form

被引：11

作者：

Balsells, J ^{[1
]}

Moyano, A ^{[1
]}

Pericas, MA ^{[1
]}

Riera, A ^{[1
]}

机构：

[1] UNIV BARCELONA,UNITAT RECERCA SINTESI ASIMETR,DEPT QUIM ORGAN,E-08028 BARCELONA,SPAIN

来源：

TETRAHEDRON-ASYMMETRY | 1997年 / 8卷 / 10期

关键词：

D O I：

10.1016/S0957-4166(97)00126-2

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Chiral acetylene dithioethers have been synthesized by the first time in enantiomerically pure form through a high yield (93-100%), one-pot procedure involving the successive treatment of trichloroethylene with three equivalents of lithium bis(trimethylsilyl)amide and two equivalents of a chiral thiol in diethyl ether solution. (C) 1997 Elsevier Science Ltd.

引用

页码：1575 / 1580

页数：6

共 50 条

[31] An efficient synthesis of enantiomerically pure diethyl 2,3-dihydroxypropylphosphonate
Wróblewski, AE
Halajewska-Wosik, A
TETRAHEDRON-ASYMMETRY, 2004, 15 (13) : 2075 - 2077
[32] A practical and efficient synthesis of enantiomerically pure di-tert-butylethanediamine
Roland, S
Mangeney, P
Alexakis, A
SYNTHESIS-STUTTGART, 1999, (02): : 228 - 230
[33] Efficient synthesis of enantiomerically pure α-alkyl cyclopropanecarbonitrile derivatives from pyrazolines
Ruano, JLG
de Diego, SAA
Martín, MR
Torrente, E
Castro, AMM
ORGANIC LETTERS, 2004, 6 (26) : 4945 - 4948
[34] SYNTHESIS OF AN ENANTIOMERICALLY PURE INDOLOSESQUITERPENE
SARRAGIOTTO, MH
GOWER, AE
MARSAIOLI, AJ
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1989, (03): : 559 - 562
[35] Efficient chemoenzymatic synthesis of enantiomerically pure β-heterocyclic amino acid derivatives
Rolland-Fulcrand, V
Haroune, N
Roumestant, ML
Martinez, J
TETRAHEDRON-ASYMMETRY, 2000, 11 (23) : 4719 - 4724
[36] An efficient synthesis of enantiomerically pure unnatural aryl glycinols and aryl glycines
Ku, Hui-Young
Jung, Junyang
Kim, Soo-Hyun
Kim, Hee Yeon
Ahn, Kyo Han
Kim, Sung-Gon
TETRAHEDRON-ASYMMETRY, 2006, 17 (07) : 1111 - 1115
[37] An efficient synthesis of an enantiomerically pure phosphonate analogue of L-GABOB
Wróblewski, AE
Halajewska-Wosik, A
TETRAHEDRON-ASYMMETRY, 2003, 14 (21) : 3359 - 3363
[38] Synthesis of (R)-quinuclidine-2-carboxylic acid in enantiomerically pure form
Etayo, Pablo
Badorrey, Ramon
Diaz-de-Villegas, Maria D.
Galvez, Jose A.
TETRAHEDRON LETTERS, 2008, 49 (14) : 2251 - 2253
[39] AN EFFICIENT APPROACH TO ENANTIOMERICALLY PURE FLUORHYDRINS
BRAVO, P
RESNATI, G
TETRAHEDRON LETTERS, 1987, 28 (41) : 4865 - 4866
[40] SYNTHESIS OF THE ZIEGLER KEY INTERMEDIATE AND RELATED PRECURSORS FOR THE SYNTHESIS OF FORSKOLIN AND ERIGEROL IN ENANTIOMERICALLY PURE FORM
PREITE, MD
RUVEDA, EA
SYNTHETIC COMMUNICATIONS, 1994, 24 (19) : 2809 - 2825

← 1 2 3 4 5 →