Solvothermal synthesis of zirconia and yttria-stabilized zirconia nanocrystalline particles

被引：5
|
作者：
Wang, Xin M. [1 ]
Xiao, Ping [1 ]
机构：
[1] Univ Manchester, Ctr Mat Sci, Manchester M1 7HS, Lancs, England
来源：
JOURNAL OF MATERIALS RESEARCH | 2007年 / 22卷 / 01期
基金：
英国工程与自然科学研究理事会;
关键词：
D O I：
10.1557/JMR.2007.0012
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A solvothermal method was used to prepare zirconia and yttria-stabilized zirconia (YSZ) particles using zirconium hydroxide and yttrium hydroxide particles as precursors and ethanol or isopropanol as reaction media. The particle properties were characterized with x-ray diffractometry, scanning electron microscopy, transmission electron microscopy, thermal analysis, laser particle-size analysis, nitrogen adsorption (Brunauer-Emmett-Teller method) and Zeta potential analysis. Cubic/tetragonal ZrO2 and YSZ nanocrystals with crystallite size around 5 nm were obtained. The effect of different hydroxide precursors, attrition milling of hydroxide precursors, solvothermal processing conditions, and mineralizer was investigated and discussed by referring to the crystallization process of zirconium hydroxides.
引用
收藏
页码：46 / 55
页数：10
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