Fabrication of Y2O3 microspheres by homogeneous precipitation method

被引:1
|
作者
Song, Li [1 ]
Li, Junwei [1 ]
Zhang, Min [2 ]
Zhang, Baohang [1 ]
Wang, Jiaxin [1 ]
Li, Zhehui [1 ]
机构
[1] Tianjin Chengjian Univ, Sch Mat Sci & Engn, Tianjin 300384, Peoples R China
[2] Logist Univ Chinese Peoples Armed Police Forces, Dept Sci Res, Tianjin 300309, Peoples R China
基金
中国博士后科学基金;
关键词
LUMINESCENT PROPERTIES;
D O I
10.1049/mnl.2016.0663
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Y2O3 microspheres were obtained via homogeneous precipitation method. Y2O3 microspheres with different sizes and morphologies were prepared by adjusting the reaction temperature, the concentration of ytterbium nitrate and urea ( H2NCONH2), and the amount and species of surfactants. The structure and morphology of the as-obtained Y2O3 were analysed by using X-ray diffraction, scanning electron microscopy and transmission electron microscopy, and the results showed that the sample showed the optimal microscopy when it was prepared at 80 degrees C with the concentration of ytterbium nitrate, H2NCONH2 and betaine fixed at 0.01 M, 0.04 M and 4 g/l, respectively. Moreover, the as-prepared samples were uniform and smooth-surfaced.
引用
收藏
页码:214 / 216
页数:3
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