An expeditious one-pot synthesis of thiiranes from α-halo ketones in solvent-free conditions using microwaves

被引：20
|
作者：
Yadav, LDS [1 ]
Kapoor, R [1 ]
机构：
[1] Univ Allahabad, Dept Chem, Allahabad 211002, Uttar Pradesh, India
来源：
SYNTHESIS-STUTTGART | 2002年 / 16期
关键词：
alpha-hatoketones; thiiranes; stereoselective synthesis; microwaves; solvent free; alumina supported;
D O I：
10.1055/s-2002-35222
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Thiiranes are obtained in excellent yields and with high diastereoselectivity upon microwave irradiation of a mixture of alpha-haloketones, O,O-diethyl hydrogen phosphorodithioate and alumina-supported sodium borohydride in solvent-free conditions.
引用
收藏
页码：2344 / 2346
页数：3
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