One-dimensional Coordination Polymer as New Precursor for Preparation of Fe2O3 Nano-particles

被引：9

作者：

Mehrani, Azadeh ^{[1
]}

Morsali, Ali ^{[1
]}

机构：

[1] Tarbiat Modares Univ, Fac Sci, Dept Chem, Tehran, Iran

来源：

JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2011年 / 21卷 / 03期

关键词：

4 '-(4-Pyridyl)-2,2 ':6 ',2 '-terpyridine; Fe2O3; Nano-particles; ALPHA-FE2O3; NANOSTRUCTURES; HEMATITE; SIZE;

D O I：

10.1007/s10904-011-9476-8

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

A Fe(II) one-dimensional coordination polymer, [Fe(pyterpy)(2)](SCN)(2).MeOH (1), which pyterpy is 4'-(4-Pyridyl)-2,2':6',2'-terpyridine, has been synthesized by using branched tube and characterized by elemental analysis, X-ray powder diffraction (XRD) and IR spectroscopy. Iron(III) oxide nano-particles were obtained by thermolysis of compound 1 in oleic acid (surfactant) at 286 A degrees C under air atmosphere. The Fe2O3 nano-particles were characterized by XRD and scanning electron microscopy. This study demonstrates that the Fe(II) coordination polymers are suitable precursors for the simple one-pot preparation of iron oxide nano-materials.

引用

页码：476 / 479

页数：4

共 50 条

[41] Formation and characteristics of Fe2O3 nano-particles in doped low pressure H2/O2/Ar flames
Janzen, C
Roth, P
[J]. COMBUSTION AND FLAME, 2001, 125 (03) : 1150 - 1161
[42] Preparation of α-Fe2O3 nanoparticles from a nonaqueous precursor medium
Deb, P
Basumallick, A
Chatterjee, P
Sengupta, SP
[J]. SCRIPTA MATERIALIA, 2001, 45 (03) : 341 - 346
[43] One-dimensional quantum-confinement effect in α-Fe2O3 ultrafine nanorod arrays
Vayssieres, L
Sathe, C
Butorin, SM
Shuh, DK
Nordgren, J
Guo, JH
[J]. ADVANCED MATERIALS, 2005, 17 (19) : 2320 - +
[44] THE EFFECT OF NANO-PARTICLES ON THE ONE-DIMENSIONAL SHOCK COMPACTION OF AL-MNO2-EPOXY MIXTURES
Fraser, A.
Borg, J. P.
Jordan, J. L.
[J]. SHOCK COMPRESSION OF CONDENSED MATTER - 2009, PTS 1 AND 2, 2009, 1195 : 61 - +
[45] Monodispersed Fe3O4-Dextra nano-particles:: Preparation and super paramagnetic property
Yang, YD
Lang, Y
[J]. CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2005, 21 (01) : 133 - 136
[46] PREPARATION AND CHARACTERIZATION OF FE2O3 MICRO-NANO MATERIALS
Wu, Shitao
Wu, Guoxi
[J]. INTERNATIONAL JOURNAL OF HEAT AND TECHNOLOGY, 2015, 33 (02) : 57 - 62
[47] Preparation and combustion properties of α-Fe2O3 coated Zr particles
Lv, Baoliang
Xu, Yao
Hou, Bo
Wu, Dong
Sun, Yuhan
[J]. MATERIALS RESEARCH BULLETIN, 2008, 43 (10) : 2769 - 2777
[48] Preparation and characterization of α-Fe2O3 nanometer particles of different appearance
Li, Qiao-lin
Jing, Hong-xia
Cui, Li-li
Ye, Yun
Wang, Ya-kun
[J]. ADVANCES IN COMPOSITE MATERIALS AND STRUCTURES, PTS 1 AND 2, 2007, 334-335 : 997 - +
[49] Characteristics of Fe2O3/SiO2 nano-composites particles prepared by a diffusion flame with premixed precursor
Ahn, KH
Ahn, JH
Jeon, KS
Choa, YH
[J]. DESIGNING, PROCESSING AND PROPERTIES OF ADVANCED ENGINEERING MATERIALS, PTS 1 AND 2, 2004, 449-4 : 1173 - 1176
[50] Fe2O3 nano particles embedded Fe2O3/BP2000 composite for Li-S battery
Lu, Yi
Liu, Tao
[J]. JOURNAL OF POROUS MATERIALS, 2024, 31 (05) : 1801 - 1809

← 1 2 3 4 5 →