One-dimensional Coordination Polymer as New Precursor for Preparation of Fe2O3 Nano-particles

被引：9
|
作者：
Mehrani, Azadeh [1 ]
Morsali, Ali [1 ]
机构：
[1] Tarbiat Modares Univ, Fac Sci, Dept Chem, Tehran, Iran
来源：
JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2011年 / 21卷 / 03期
关键词：
4 '-(4-Pyridyl)-2,2 ':6 ',2 '-terpyridine; Fe2O3; Nano-particles; ALPHA-FE2O3; NANOSTRUCTURES; HEMATITE; SIZE;
D O I：
10.1007/s10904-011-9476-8
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
A Fe(II) one-dimensional coordination polymer, [Fe(pyterpy)(2)](SCN)(2).MeOH (1), which pyterpy is 4'-(4-Pyridyl)-2,2':6',2'-terpyridine, has been synthesized by using branched tube and characterized by elemental analysis, X-ray powder diffraction (XRD) and IR spectroscopy. Iron(III) oxide nano-particles were obtained by thermolysis of compound 1 in oleic acid (surfactant) at 286 A degrees C under air atmosphere. The Fe2O3 nano-particles were characterized by XRD and scanning electron microscopy. This study demonstrates that the Fe(II) coordination polymers are suitable precursors for the simple one-pot preparation of iron oxide nano-materials.
引用
收藏
页码：476 / 479
页数：4
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