Room temperature synthesis in liquid ammonia of tin sulfide

被引：0

作者：

Shaw, GA ^{[1
]}

Parkin, IP ^{[1
]}

机构：

[1] UNIV LONDON UNIV COLL,DEPT CHEM,LONDON WC1H 0AJ,ENGLAND

来源：

MAIN GROUP METAL CHEMISTRY | 1996年 / 19卷 / 08期

关键词：

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Reaction of elemental tin with sulfur in liquid ammonia at room temperature affords an intimate mixture of X-ray amorphous metal sulfides (SnS, SnS2) and a trace of tin metal. Thermolysis of this material at 300-350 degrees C for 2 hrs. produced crystalline tin (II) sulfide (SnS-Herzenbergite). Products were characterised by elemental analysis, FT-IR and Raman spectroscopy, Sn-119 NMR, X-ray powder diffraction, Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Analysis (EDXA).

引用

页码：499 / 502

页数：4

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