Hydrothermal synthesis and crystal structure of two new lanthanide coordination polymers with 1,2-phenylenediacetate

被引：15

作者：

Li, Xia ^{[2
]}

Wang, Chunyan ^{[2
]}

Zheng, Xiangjun ^{[1
]}

Zou, Yingquan ^{[1
]}

机构：

[1] Beijing Normal Univ, Dept Chem, Beijing 100875, Peoples R China

[2] Capital Normal Univ, Dept Chem, Beijing 100037, Peoples R China

来源：

JOURNAL OF COORDINATION CHEMISTRY | 2008年 / 61卷 / 07期

关键词：

lanthanide coordination polymers; 1,2-phenylenediacetate; hydrothermal synthesis; crystal structure;

D O I：

10.1080/00958970701502003

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two new compounds {[Ln(2)(1,2-pda)(3)(H2O)(2)]center dot 2H(2)O}n (1,2-H(2)pda = 1,2-phenylenediacetic acid, Ln = Tb, 1; Ho, 2) were prepared by hydrothermal reaction and characterized by X-ray crystallography. The Ln(3+) is nine-coordinate by eight oxygen atoms of six 1,2-pda ligands and one oxygen of water. Ln(3+) ions are bridged by 1,2-pda ligands via bridging/chelating-bridging pentadentate and chelating-bridging/chelating-bridging hexadentate coordination to form 3-D framework structures. Complex 1 emits strong green fluorescence corresponding to D-5(4) -> F-7(j) (j = 6-3) transitions of the Tb3+.

引用

页码：1127 / 1136

页数：10

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