Sintering by SPS of ultrafine TiCxN1-x powders obtained using mechanically induced self sustaining reaction.

被引：0

作者：

Borrell, A. ^{[1
]}

Fernandez, A. ^{[2
]}

Torrecillas, R. ^{[1
]}

Cordoba, J. M. ^{[3
]}

Aviles, M. A. ^{[3
]}

Gotor, F. J. ^{[3
]}

机构：

[1] CSIC, CINN, Llanera 33428, Asturias, Spain

[2] Fdn ITMA, Llanera 33428, Asturias, Spain

[3] CSIC US, Inst Ciencia Mat Sevilla, Seville 41092, Spain

来源：

BOLETIN DE LA SOCIEDAD ESPANOLA DE CERAMICA Y VIDRIO | 2010年 / 49卷 / 05期

关键词：

Ti(C; N); mechanically induced self sustaining reaction (MSR); spark plasma sintering (SPS); microstructure; mechanical properties; TITANIUM CARBONITRIDE PHASES; REDUCTION; TIO2;

D O I：

暂无

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

In this work high purity and nanometer character titanium carbonitride TiCxN1-x powders were obtained by mechanically induced self sustaining reaction (MSR) in a high-energy planetary ball mill, from a mixture of titanium with graphite or carbon nanofiber (CNFs) in a nitrogen atmosphere. A promising method for developing these materials is the coupling of the MSR with SPS sintering technique. The product is sintered at 1400 degrees C and 1700 degrees C, obtaining a completely dense monolithic ceramic (>99% t.d). In this work, the influence of SI'S treatment and carbon precursor on material microstructures was studied and the main mechanical properties of the end material were evaluated.

引用

页码：357 / 360

页数：4

共 15 条

[1] Spark Plasma Sintering of Ultrafine TiCxN1-x Powders Synthesized by a Mechanically Induced Self-Sustaining Reaction
Borrell, Amparo
Fernandez, Adolfo
Torrecillas, Ramon
Cordoba, Jose M.
Aviles, Miguel A.
Gotor, Francisco J.
[J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2010, 93 (08) : 2252 - 2256
[2] Effects of additives on the synthesis of TiCxN1-x by a solid-gas mechanically induced self-sustaining reaction
Chicardi, E.
Gotor, F. J.
Alcala, M. D.
Cordoba, J. M.
[J]. CERAMICS INTERNATIONAL, 2018, 44 (07) : 7605 - 7610
[3] Influence of milling parameters on the solid-gas synthesis of TiCxN1-x by mechanically induced self-sustaining reaction
Chicardi, E.
Gotor, F. J.
Alcala, M. D.
Cordoba, J. M.
[J]. POWDER TECHNOLOGY, 2017, 319 : 12 - 18
[4] Creep behavior of TiCxN1-x-CoTi cermets synthesized by mechanically induced self-sustaining reaction
Morales-Rodriguez, A.
Gallardo-Lopez, A.
Dominguez-Rodriguez, A.
Cordoba, J. M.
Aviles, M. A.
Gotor, F. J.
[J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2011, 31 (03) : 299 - 302
[5] New production of TiCxN1-x-based cermets by one step mechanically induced self-sustaining reaction:: Powder synthesis and pressureless sintering
Cordoba, J. M.
Alcala, M. D.
Aviles, M. A.
Sayagues, M. J.
Gotor, F. J.
[J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2008, 28 (10) : 2085 - 2098
[6] Spark plasma sintering of TiyNb1-yCxN1-x monolithic ceramics obtained by mechanically induced self-sustaining reaction
Borrell, Amparo
Dolores Salvador, Maria
Garcia-Rocha, Victoria
Fernandez, Adolfo
Chicardi, Ernesto
Gotor, Francisco J.
[J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2012, 543 : 173 - 179
[7] Bulk TiCxN1-x-15%Co cermets obtained by direct spark plasma sintering of mechanochemical synthesized powders
Borrell, Amparo
Dolores Salvador, Maria
Rocha, Victoria G.
Fernandez, Adolfo
Angel Aviles, Miguel
Gotor, Francisco J.
[J]. MATERIALS RESEARCH BULLETIN, 2012, 47 (12) : 4487 - 4490
[8] The effect of aluminum substitution on the mechanically induced self-sustaining reaction of molybdenum-silicon powders
Takacs L.
[J]. International Journal of Self-Propagating High-Temperature Synthesis, 2013, 22 (1) : 41 - 45
[9] Tuning the excitation wavelength of luminescent Mn2+-doped ZnSxSe1-x obtained by mechanically induced self-sustaining reaction
Avilés, M.A.
Gotor, F.J.
[J]. Optical Materials, 2021, 117
[10] Tuning the excitation wavelength of luminescent Mn2+-doped ZnSxSe1-x obtained by mechanically induced self-sustaining reaction
Avil, M. A.
Gotor, F. J.
[J]. OPTICAL MATERIALS, 2021, 117

← 1 2 →