Synthesis of Monodisperse Silver Nanoparticles by Sonolysis of Silver Carboxylates

被引：3
|
作者：
Veith, Michael [1 ,2 ]
Moh, Karsten [1 ]
Cavelius, Christian [1 ]
机构：
[1] INM, Leibniz Inst New Mat, D-66123 Saarbrucken, Germany
[2] Univ Saarland, D-66123 Saarbrucken, Germany
来源：
ADVANCED ENGINEERING MATERIALS | 2012年 / 14卷 / 09期
关键词：
THERMAL-DECOMPOSITION; COLLOIDAL SOLUTION; FABRICATION; PARTICLES;
D O I：
10.1002/adem.201200111
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Monodisperse, crystalline silver nanoparticles are synthesized by sonolytically assisted decomposition of silver oxalate and oleate precursors in dibenzylether. Oleic acid and oleylamine are used as capping agents. The diameters of the obtained particles vary from 6 to 10?nm depending on the sonification time and the precursor material. The particles are stable in non-polar media. A 2D and 3D assembly of the as-prepared nanoparticles is observed. Particle sizes and dispersities are characterized by transmission electron microscopy and image analysis. The decomposition characteristics of the different precursor compounds are investigated using UVVis spectroscopy and thermogravimetry.
引用
收藏
页码：825 / 829
页数：5
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