Nitropyridines. 7. Synthesis of nitropyridines from nitro-malonic dialdehyde

被引：5

作者：

Sagitullina, G. P. ^{[1
]}

Garkushenko, A. K. ^{[1
]}

Silina, E. O. ^{[1
]}

Sagitullin, R. S. ^{[1
]}

机构：

[1] FM Dostoevsky Omsk State Univ, Omsk 64077, Russia

来源：

CHEMISTRY OF HETEROCYCLIC COMPOUNDS | 2009年 / 45卷 / 08期

关键词：

enamines; nitromalonic dialdehyde; nitropyridines; SODIUM NITROMALONALDEHYDE; CONDENSATION;

D O I：

10.1007/s10593-009-0366-8

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Cyclocondensation of sodium nitromalone dialdehyde with different enamines gave 3-acetyl(benzoyl, cyano, cyclopropanoyl, carbethoxy)-2-methyl(phenyl)-5-nitropyridines. With the aim of increasing the yield of pyridines we have activated the nitromalonic dialdehyde through acylation of its enol form.

引用

页码：948 / 951

页数：4

共 50 条

[31] FROM PENICILLIN TO PENEM AND CARBAPENEM .7. SYNTHESIS AND ANTIBACTERIAL ACTIVITY OF PENEM DERIVATIVES
FUJIMOTO, K
IWANO, Y
HIRAI, K
CHEMICAL & PHARMACEUTICAL BULLETIN, 1986, 34 (03) : 999 - 1014
[32] BIOSYNTHESIS OF THE PURINES .7. SYNTHESIS OF NUCLEOTIDES FROM BASES BY PARTIALLY PURIFIED ENZYMES
KORN, ED
REMY, CN
WASILEJKO, HC
BUCHANAN, JM
JOURNAL OF BIOLOGICAL CHEMISTRY, 1955, 217 (02) : 875 - 883
[33] STUDIES ON NITRO SUGARS .7. SYNTHESIS OF METHYL 2,3,5-TRIACETAMIDO-2,3,5-TRIDEOXY-BETA-D-PENTOFURANOSIDES VIA NITRO-OLEFIN
TAKAMOTO, T
TANAKA, H
KAWAHARA, T
SUDOH, R
CHEMISTRY LETTERS, 1976, (02) : 137 - 140
[34] TERPENES FROM HIGHER PLANTS .7. STRUCTURE AND SYNTHESIS OF A THYMOL DERIVATIVE FROM HELENIUM SPECIES
BOHLMANN, F
SCHULZ, J
BUHMANN, U
TETRAHEDRON LETTERS, 1969, (53) : 4703 - &
[35] SYNTHESIS OF THIAZOLIDONES OF BIOLOGICAL INTEREST .7. SYNTHESIS OF N-SUBSTITUTED RHODAMINES FROM THIOCYANOACETATES (FUNGICIDES)
ZUBENKO, VG
TURKEVICH, NM
ZHURNAL OBSHCHEI KHIMII, 1957, 27 (12): : 3275 - 3278
[36] THE SYNTHESIS OF SUGARS FROM SIMPLER SUBSTANCES .7. ENZYMIC SYNTHESIS OF 5-DEOXY-D-XYLULOSE
GORIN, PAJ
HOUGH, L
JONES, JKN
JOURNAL OF THE CHEMICAL SOCIETY, 1953, (JUL): : 2140 - 2142
[37] The synthesis of 7-nitro-2-alkyl-4-ketodihydro-quinazolines from 4-nitroacetanthranilic acid, and from 4-nitro-acetanthranil.
Bogert, MT
Steiner, SH
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1905, 27 (10) : 1327 - 1331
[38] SYNTHESIS OF POTENTIAL ANTICANCER AGENTS .7. NUCLEOSIDES DERIVED FROM L-RHAMNOPYRANOSE
BAKER, BR
HEWSON, K
JOURNAL OF ORGANIC CHEMISTRY, 1957, 22 (08): : 959 - 966
[39] PHOTOCHEMICAL NITRATION BY TETRANITROMETHANE .7. MODE OF FORMATION OF THE NITRO SUBSTITUTION PRODUCTS FROM 1,4-DIMETHYLNAPHTHALENE IN DICHLOROMETHANE AND ACETONITRILE
EBERSON, L
HARTSHORN, MP
RADNER, F
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1992, (10): : 1799 - 1806
[40] ANTIBIOTIC MODELS .7. DIASTEREOSELECTIVE SYNTHESIS OF A RHODOMYCINONE MODEL FROM DEUTERIUM-GLUCOSE
DYONG, I
HAGEDORN, HW
THIEM, J
LIEBIGS ANNALEN DER CHEMIE, 1986, (03): : 551 - 563

← 1 2 3 4 5 →