GC-MS analysis of organic compounds in wastewater and sewage sludge

被引：20
|
作者：
Ligon, Axel Patrick [1 ]
Zuehlke, Sebastian [1 ]
Spiteller, Michael [1 ]
机构：
[1] Univ Dortmund, INFU, D-44221 Dortmund, Germany
来源：
JOURNAL OF SEPARATION SCIENCE | 2008年 / 31卷 / 01期
关键词：
mass spectrometry; multimethod; persistent organic pollutants; wastewater treatment plants;
D O I：
10.1002/jssc.200700361
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A multimethod based on liquid-liquid extraction and solid-liquid extraction for the analysis of persistent organic pollutants in water and sludge from sewage treatment plants has been established. Traces of 22 organic compounds used in industry and personal care products (PCPs) were analyzed by GC/MS. The LODs for the analytes were less than 2.3 ng/L for wastewater and 31 mu g/kg (dry weight matter) for sewage sludge. Satisfactory recoveries (70-130%) were achieved. The validated method permits the analysis of water and sludge samples at various stages of the treatment from different sewage treatment plants. Thus, the distribution between water and sludge as well as the dissipation of the compounds analyzed were balanced. By this means, the efficiency of different wastewater treatment plants (WWTPs) can be evaluated and measures can be taken to optimize the treatment process at different stages.
引用
收藏
页码：143 / 150
页数：8
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