A versatile method for the conversion of aldoximes to nitriles using silica gel/thionyl chloride

被引：6

作者：

Kazemi, F ^{[1
]}

Kiasat, AR ^{[1
]}

Fadavipoor, E ^{[1
]}

机构：

[1] Chamran Univ, Coll Sci, Chem Dept, Ahvaz, Iran

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2004年 / 179卷 / 02期

关键词：

aldoxime; nitrile; silica gel; thionyl chloride;

D O I：

10.1080/10426500490262586

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A simple convenient procedure for dehydration of aldoximes has been developed using silica gel/thionyl chloride in heterogeneous conditions. The method has been found to be effective for a wide range of aromatic oximes.

引用

页码：433 / 436

页数：4

共 50 条

[1] A conversion of aldoximes to nitriles using dabco/thionyl chloride complex
Kazemi, F
Kiasat, AR
[J]. INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2003, 42 (06): : 1540 - 1543
[2] VERSATILE METHOD FOR CONVERSION OF ALDOXIMES TO NITRILES USING SELENIUM DIOXIDE
SOSNOVSKY, G
KROGH, JA
[J]. SYNTHESIS-STUTTGART, 1978, (09): : 703 - 705
[3] Thionyl chloride-benzotriazole: An efficient system for transformation of aldoximes to nitriles
Chaudhari, SS
Akamanchi, KG
[J]. SYNTHETIC COMMUNICATIONS, 1999, 29 (10) : 1741 - 1745
[4] A NEW METHOD FOR THE CONVERSION OF ALDOXIMES INTO NITRILES WITH ZEOLITES
RAO, MN
KUMAR, P
GARYALI, K
[J]. ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1989, 21 (02) : 230 - 232
[5] Synthesis of nitriles from aldoximes using silica gel as catalyst under microwave irradiation
Dewan, SK
Singh, R
[J]. SYNTHETIC COMMUNICATIONS, 2003, 33 (17) : 3085 - 3088
[6] A MILD, HIGH-YIELD CONVERSION OF ALDOXIMES INTO NITRILES USING TRICHLOROACETYL CHLORIDE TRIETHYLAMINE
SAEDNYA, A
[J]. SYNTHESIS-STUTTGART, 1983, (09): : 748 - 749
[7] A NEW METHOD FOR CONVERSION OF ALDOXIMES INTO NITRILES - USE OF CHLOROTHIONOFORMATES
CLIVE, DLJ
[J]. JOURNAL OF THE CHEMICAL SOCIETY D-CHEMICAL COMMUNICATIONS, 1970, (16): : 1014 - &
[8] Silica gel/thionyl chloride: An efficient reagent for the conversion of alcohols to symmetrical dialkyl sulfites
Kazemi, F
Kiasat, AR
Fadavipoor, E
[J]. ASIAN JOURNAL OF CHEMISTRY, 2006, 18 (02) : 973 - 976
[9] A convenient conversion of aldoximes to nitriles using a polymer supported system
Tamami, B
Kiasat, AR
[J]. SYNTHETIC COMMUNICATIONS, 2000, 30 (02) : 235 - 242
[10] A new, mild, neutral and inexpensive method for conversion of aldoximes to nitriles using anhydrous ferric sulphate
Desai, DG
Swami, SS
Mahale, GD
[J]. SYNTHETIC COMMUNICATIONS, 2000, 30 (09) : 1623 - 1625

← 1 2 3 4 5 →